FCC ID: XGQFCCBMA1000 Moisture Measuring System

 

Concentration Meter DynFAS MW Hardware Manual User's Guide ID No. 54877BA2 Rev. No. 00 01.07.2009 The units supplied should not be repaired by anyone other than BMA Schaltanlagen Service engineers or technicians by BMA Schaltanlagen. In case of operation trouble, please address to our central service department. The complete users guide consists of two parts, namely the hardware and software instruc-

tions. installation The hardware manual comprises:

mechanical components

electrical installation

technical data

electrical and mechanical drawings The software manual comprises:

operation of the control unit

parameter description

basic setting

calibration

error messages The present part is the hardware instruction. Subject to change without prior notice. BMA Schaltanlagen GmbH Am Alten Bahnhof 5 38122 Braunschweig Germany Tel. +49 531 804 261 Fax +49 531 804 269 schaltanlagen@bma-de.com www.bma-worldwide.com DynFAS MW Table of Contents Table of Contents Chapter 1. Safety Instructions 1.1 Identification and warning notices 1.2 General Instructions 1.3 General Safety Instructions Chapter 2. General Information 2.1 Use and Function 2.2 Frequency approval 2.3 Intended Use 2.4 Definitions Chapter 3. System Description 3.1 Principle of Measurement 3.2 Calculation of Measured Values 3.3 Temperature Compensation 3.4 Mechanical Components 3.4.1 Control Units 3.4.2 Flow Cell 3.4.3 Container Probe 3.4.4 High-Frequency Cable 3.5 Pipeline Measurement Configuration 3.6 Container Measurement Configuration Chapter 4. Getting Started 4.1 Transport 4.2 Installation 4.2.1 Flow Cell Installation 4.2.2 Container Probe Installation 4.2.3 Installing the Control Unit 4.3 Connecting the Control Unit 4.3.1 Connecting the HF Cable 4.3.2 Pin Configuration of the Connector Strip 4.3.3 Digital Outputs, Relays Chapter 5. Service Instructions 5.1 General Information 5.2 Wearing Parts 5.3 Instrument Cleaning 5.4 Battery 5.5 Fuse Replacement Chapter 6. Technical Data 6.1 Control Unit 6.2 Technical Data Sensors 6.3 Technical Data HF-Cable 6.4 Format of Serial Data Output RS 232 and RS 485 Page 7 7 8 9 11 11 12 14 15 16 16 17 18 19 20 23 24 28 30 31 32 32 32 32 34 36 37 37 40 44 45 45 45 45 46 46 47 47 50 52 53 DynFAS MW 5 Table of Contents Chapter 7. Certificates 7.1 EC Declaration of Conformity 7.2 Frequency Approval Chapter 8. Technical Drawings 8.1 Dimensional Drawing of Control Unit Housing 8.1.1 Control Unit Standard CS-100 8.1.2 Control Unit High Dynamic CH-200 8.2 Electrical Wiring Diagram 8.3 Dimensional Drawings Flow Cells 8.3.1 Type FC-050-016 8.3.2 Type FC-065-040 8.3.3 Type FC-080-016 8.3.4 Type FC-100-016 8.3.5 Type FC-150-016 8.3.6 Type FC-020-150 8.3.7 Type FC-025-300 8.3.8 Type FC-030-150 8.3.9 Type FC-040-150 8.3.10 Type FC-060-150 8.4 Dimensional Drawings Probes 8.4.1 Type P-065-006 8.4.2 Type P-080-016 8.4.3 Type P-100-016 8.4.4 Type P-150-016 8.4.5 Type P-025-150 8.4.6 Type P-030-150 8.4.7 Installation Situation in Pipelines 8.5 Dimensional Drawings Flush Probes 8.5.1 Type PF-065-006 8.5.2 Type PF-080-016 8.5.3 Type PF-100-016 8.5.4 Type PF-150-016 8.5.5 Type PF-025-150 8.5.6 Installation Situation in Pipelines 8.6 Installation Sheets for DynFAS MW (Probe) 8.7 Installation Sheets for DynFAS MW (Flush Probe) 6 55 55 57 63 63 63 64 65 66 66 67 68 69 70 71 72 73 74 75 76 76 77 78 79 80 81 82 83 83 84 85 86 87 88 89 91 DynFAS MW Chapter 1 Safety Instructions Chapter 1. Safety Instructions 1.1 Identification and warning notices The term BMA Schaltanlagen in this Users Manual stands for the company BMA Schaltanlagen GmbH. Please observe the warnings and safety instructions given in this Users Manual to rule out physical injury and property damage. They are identified by the following symbols: DANGER, WARNING, CAUTION or NOTICE. Indicates an imminently dangerous condition. Failure to follow the instructions will lead to death or serious injury. Indicates a potentially dangerous condition. Failure to follow the instructions may lead to death or serious injury. Indicates a potentially dangerous condition. Failure to follow the instructions may lead to slight injury or a medium-degree injury. Indicates a situation which may cause property damage if the in-

structions are not followed. IMPORTANT Paragraphs with this symbol provide important information on the product or how to work with the product. Tip Includes application tips and other useful information. Further Symbols Warning sign: no intervention, change nothing 7 DynFAS MW Chapter 1 Safety Instructions Instruction: Disconnect from mains supply Instruction: Wear safety shoes 1.2 General Instructions The most important safety measures are summarised in this op-

eration manual. It supplements the applicable regulations which have to be studied by the personnel in charge. Please keep in mind:

the national safety and accident prevention regulations

the national installation regulations (e.g. EN 60079)

the generally accepted engineering rules

the information on transportation, installation, operation, ser-

vice and maintenance

the safety instructions and information in this Users Manual and the enclosed technical drawings and wiring diagrams

the characteristic data, limit values and the information on the operating and environmental conditions on the type labels and data sheets

the signs on the devices 8 DynFAS MW Chapter 1 Safety Instructions 1.3 General Safety Instructions IMPORTANT The instrument housings are protected according to protection type IP 65 and are suitable for outdoor application. The instru-

ment has been tested by the manufacturer and is delivered in a condition that allows safe and reliable operation. The measuring systems have to be protected against direct sun rays and rain during outdoor applications e. g. by a suitable pro-

tective cover. IMPORTANT Never change the installation and the parameter settings without a full knowledge of these operating instructions, as well as a full knowledge of the behavior of the connected controller and the possible influence on the operating process to be controlled. The systems may be used only in technically good order and only according to regulations!

Only authorized persons who have been trained, have the proper qualification and have received the necessary instructions may work with the systems! Installations and modifications on the sys-

tems which may affect the operational safety are not permitted!

IMPORTANT All systems components require non corrosive ambient conditions during transport, storage and starting up. Electrical shock hazard:

Disconnect power to rule out any contact with live parts during installation and when servicing. Turn off power supply before opening the instrument. NEVER work on open and live instruments. Ambient conditions DynFAS MW 9 Chapter 1 Safety Instructions Attention! Possible danger, damage to property! Concerns the sys-

tem type CH-200-024 Control Unit High Dynamic 24 V DC (Id.-No. 54878-02):

When connecting the 24 V DC auxiliary power, the + and Poles should be connected correctly. There is no reverse voltage protec-

tion!

Spare fuses must match the rating specified by the device manu-

facturer. Short-circuiting or manipulation is not permitted. IMPORTANT The DynFAS MW and all ancillary units have to be connected to mains via grounded connection. IMPORTANT The concentration measuring system DynFAS MW is to be serviced and repaired solely by qualified persons. Persons are qualified if they have acquired adequate knowledge in the area concerned in the course of their professional education, and if they are familiar with the pertinent national occupational safety regulations, accident prevention regulations, directives and acknowledged rules of technology. They must be capable of as-

sessing the result of their work safely; moreover, they need to be familiar with the contents of this Users Manual. IMPORTANT If liquid gets inside the instrument, cut off the power supply. The instrument has to be checked and cleaned by an authorized ser-

vice center. Qualified Persons 10 DynFAS MW Chapter 2 General Information Chapter 2. General Information 2.1 Use and Function The DynFAS MW has been designed as a concentration measuring system and may only be used for this purpose. If it is used in any manner, which is not described in this users manual, the protec-

tion of the device is impaired and all warranty claims are void. BMA Schaltanlagen only guarantees that the devices comply with the published specifications. The DynFAS MW may only be installed in an undamaged, dry and clean condition. Alteration work and modification of the system components are not permitted. The DynFAS MW does not qualify as a safety regulated measure-

ments. The standards and regulations customary to the DynFAS MW are listed in the system instructions in chapter 2.2 frequency approval and in chapter 7.1 EC-conformity certificate. The degree of protection of the DynFAS MW according to IEC 60529 is max. IP 65. The following is contrary to the intended use and, therefore, has to be prevented:

Use under other conditions and prerequisites than those speci-

fied by the manufacturer in the technical documents, data sheets, operating and installation instructions and in other spe-

cifications.

Use after repair by persons who have not been authorized by BMA Schaltanlagen.

Use in a damaged or corroded state.

Operation with open or inadequately closed cover.

Operation with inadequately tightened adapters and screwed cable glands.

Operation without observing the safety precautions defined by the manufacturer.

Tampering with or bypassing existing safety installations. Authorized persons are persons, who are foreseen for certain ac-

tivities as a consequence of statutory provisions, or who have been approved by BMA Schaltanlagen for carrying out certain activities. Conformance with standards Protection type Misuse warning Authorized Persons DynFAS MW 11 Chapter 2 General Information 2.2 Frequency approval The DynFAS MW complies with part 15 of the FCC1 Rules. These devices fulfill the requirements regarding immunity to interference and emitted interference and are licensed for operation. FCC-

Approval plates 1 FCC ... Federal Communications Commission 12 DynFAS MW Chapter 2 General Information The DynFAS MW complies with the R&TTE regulations 1999/5/EG and fulfill herein all requirements for this type of high-frequency device. The devices bear the identification of conformity according to the CE symbol, No. 0682 of the certification office. The certifi-

cate can be found in chapter 7.2 Frequency Approval. The DynFAS MW is a system for concentration measurement using microwave technology. The emitted microwaves have a very low activity and are, therefore, not at all hazardous to human beings or the environment. Also, the product is not affected at all by the microwaves. IMPORTANT The DynFAS MW has been manufactured in compliance with the safety requirements for microwave devices. If special legal provi-

sions exist regarding the use of microwaves, it will be the respon-

sibility of the user to adhere to them. IMPORTANT Any change in frequency or any other manipulation on the micro-

wave device will result in a loss of the frequency approval and will be prosecuted. The microwave modules do not include any replaceable compo-

nents and must not be opened. DynFAS MW 13 Chapter 2 General Information 2.3 Intended Use The measuring system DynFAS MW can be used to determine the concentration of nearly all materials which can be dissolved or sus-

pended in water using microwave technology. The following sensor and control unit versions are available:

1. The container probes have been designed for installation into pipelines with a nominal width of 200 mm and in containers, for example, crystallizers. The probe is installed such that both measuring rods (transmitter and receiver) are immersed into the product being measured. 2. The Flow Cell is a tubular probe, with microwave transmitter and receiver being firmly welded onto the outside of the pipe. The inside of the pipe is Teflon-coated. The flow cell is in-

stalled into the existing pipeline system inline or into a bypass. The control unit is available in two versions: The Standard Model CS-100 and the high dynamic version CH-200. The control unit CH-200 can only be used when sufficiently large microwave at-

tenuation (min. 40 dB) is present. The Standard Model CS-100 should be used for lower microwave attenuation. During operation, the concentration measuring device DynFAS MW send out electromagnetic radiation in the frequency range between 2.4 GHz and 2.5 GHz (range restrictions depending on local regu-

lations in your country). The microwaves which emerge are not dangerous to human beings and the environment (power emission

< 10 mW). The microwaves are emitted from the microwave win-

dow; the product is not changed by the microwaves. To ensure proper function of the meter, please pay attention to the following:

Tip

The material being measured must not be electrically conduc-

tive, i.e. the ohmic resistance is infinite.

The product must not contain any gas bubbles, or gas bubbles have to be compressed with adequate pressure when carrying out measurements in pipelines.

The ion concentration, e.g. salt content, has to be nearly con-

stant.

The total attenuation of microwave signals must be at least 40 dB for the control unit CH-200. For details, see Chapter 3.4.1 the control units 14 DynFAS MW Chapter 2 General Information 2.4 Definitions Attenuation Weakening of microwave signals, microwave measurement effect. Container flush probe Factory setting Container probe with flushing device. All parameters have been set to standard values by the manu-

facturer. In most cases this simplifies calibration of the device significantly. Despite factory setting, calibration always has to be performed. Flow cell Tubular probe for simple integration into the existing pipeline system. HF cable High-frequency cable. Microwaves Electromagnetic waves in a certain frequency range. Phase Phase or phase shift. Microwave measurement effect. Quad cable Combination of four HF cables of equal length in a corrugated tube. Softkeys Buttons associated with the software. TC Temperature compensation. DynFAS MW 15 Chapter 3 System Description Chapter 3. System Description 3.1 Principle of Measurement The microwaves that spread between the rods pass through the product being measured; their propagation speed is slowed down

(= phase shift) and their intensity is damped (= attenuation). Figure 3-1 illustrates the principle of measurement: the propaga-

tion speed of microwaves passing through the product being measured is slowed down (phase shift) and their intensity (at-

tenuation) is reduced, relative to a reference signal. HF- sources Transmitter Reference path Reference signal Phase comparison

--> Phase Product Receiver Amplitude comp

--> Attenuation Measured value:

Concentration %TS Measurement signal Phase shift Figure 3-1:

Schematic diagram:

Change of microwave by product Prerequisite is that the product being measured shows some dielectric properties. In general, water is a very distinct dielec-

tric fluid. The water or dry mass concentration, respectively, can therefore be determined by measuring the phase shift and/or attenuation. The concentration to be detected in the product is therefore de-

pendent in good approximation linear on phase shift and at-

tenuation. For this reason we can measure the concentration or the Brix content of the product using a linear calibration (see chapter 3.2 Calculation of Measured Values ). DynFAS MW 16 Chapter 3 System Description 3.2 Calculation of Measured Values The microwave measuring phase and attenuation are calibrated after an automatic plausibility analysis. During calibration, the phase and/or the attenuation or a concen-

tration value (or density value) are assigned by sampling. The calibration is full automatic and the sample taking is supported by the control unit. Which of the parameters, either phase, attenuation or both are used for the calibration depends on the size and interference of the measuring effect. For example, the attenuation is significantly more sensitive to electrolytic conductivity (salt content). In many cases, the mere phase measurement is recommended and is calculated in good approximation by a linear calibration as follows:

Con

C A

Con A, C concentration coefficients of respective calibration function phase The DynFAS MW allows you to calibrate, display and output two concentrations Con1 and Con2. You have to enter the calibration coefficients separately for concentration 1 and 2. For more infor-

mation please refer to the Software Manual. DynFAS MW 17 Chapter 3 System Description 3.3 Temperature Compensation Temperature compensation (TC) is necessary if the product tem-

perature varies. In general, we recommend connecting a tempera-

ture compensation, i.e. a temperature signal (0/4...20 mA or Pt 100) to the control unit and, if necessary, to enable the com-

pensation in the control unit. The control unit is designed such that the required TCs can be calculated automatically. The variation in temperature where temperature compensation becomes absolutely essential is dependent on the product and on the water content. In first approximation, 2C should be set as fluctuation limit. Tip comp meas

C C D

meas D

TC has to be carried out whenever you are working with. The TC corrects the phase and attenuation before the measured value calculation (calibration), in most applications according to the following formulae (linear compensation, additive). comp D Where meas = measured phase comp = compensated phase Dmeas = measured attenuation Dmeas = compensated attenuation C CD Depending on the selected function (additive, multiplicative, linear, quadratic), the required temperature coefficients appear on the Calibration menu. Temperature coefficients that are not used are set to zero.

= measured temperature (Tmeas) reference temp. (TRef)

= temperature coefficient

= temperature coefficient If you select two-range calibration (split concentration), separate TCs have to be entered for both concentration ranges. The coeffi-

cients are entered in the course of calibration. TC can be carried out via Pt 100 or via current input. This has to be defined on the Calibration menu. The Pt 100 temperature range is between 50C and +200C. How to work with the temperature compensation is described in detail in the Software Manual. 18 DynFAS MW Chapter 3 System Description 3.4 Mechanical Components The measurement system consists of a control unit, a probe and a set of special high frequency cables (in short HF-cable). The con-

trol unit is available in two versions: the standard model CS-100 and the high dynamic version CH-200, see Figure 3-2 and 3-3. Figure 3-2:

Control Unit Standard CS-100 Figure 3-3:

Control Unit High Dynamic CH-200 DynFAS MW 19 Chapter 3 System Description The probes are available in different versions, as pipeline and con-

tainer probe with and without flushing device (see Figure 3-4, 3-5 and 3-6). Abb. 3-4 left:

Probe Abb. 3-5 right:

Probe with Flushing Figure 3-6:

Flow Cell nominal width 50 mm 3.4.1 Control Units The control units consist of evaluation analyser with microwave unit. The microwaves are generated, received and analyzed by the microwave unit. Signal processing and communication take place in the evaluation computer. For simple operation, the measuring system includes a display, 4 softkeys and an alphanumeric keypad. Different functions are assigned to the softkeys on the display. 20 DynFAS MW Chapter 3 System Description Differences between Control Unit Standard CS-100 and Control Unit High Dynamic CH-200 The Control Unit High Dynamic CH-200, has an additional HF am-

plifier module in comparison to the standard model, whereby the wall housing is larger (dimensions see chapter 6.2 Technical Data control unit). Otherwise, the control units only differ in their appli-

cations. Higher product attenuations are allowed for the high dynamic ver-

sion of DynFAS MW. Therefore larger measuring paths can be irra-

diated, for example measuring cells of larger nominal width can be used. The application of both control units is predetermined by the product attenuation. Up to an attenuation of 50 dB, CS-100 is used and beyond, CH-200. The CH-200 generally requires an attenua-

tion of 40 dB. If this is lower, the software indicates an error mes-

sage. An RS232 interface is included on the underside of the instrument. LCD display Lock Numerical keypad Softkey buttons LEDs HF connections for signal cable reference cable and cable feed-through RS232 connection Cable feed-through M 20 and M 16 M-Rx M-Tx R-Tx R-Rx RS232 9-pole Sub-D-connector High-frequency connections High Dynamic Version CH-200 Figure 3-7:

Front view of CS-100 Figure 3-8:

Control Unit -

bottom view DynFAS MW 21 Chapter 3 System Description LEDs on the Front Panel Five LEDs on the instrument front panel indicate the instrument status. Figure 3-9:

LEDs on the front panel of the Control Unit LED RUN ERR SIG 1 SIG 2 COM Function Instrument in measurement mode Display is flashing when concentration average value is put on hold, e.g. if an error has occurred, if the measurement has been paused or stopped Error Goes out after reset or if fault has been repaired Display depending on the selected function of relay 1, possible functions: error, no product, limit value min., limit value max., measurement stopped Display depending on the selected function of relay 2, possible functions: error, no product, limit value min., limit value max., measurement stopped. Communication active, e.g. via RS 232 Terminal Block The electrical connections of the DynFAS MW are located on a con-

nector strip in the wall housing. The terminal block is accessible from the front after you have opened the cover. There, you also find the power cut-off switch and the fuses. The high-frequency connections are located on the outside of the housing. All other elements, especially the live elements (on the motherboard) are provided with a protection cap. 22 DynFAS MW Chapter 3 System Description 3.4.2 Flow Cell The flow cells are available with nominal widths from 50 to 150 mm (see Figure 3-10) and different flanges. For technical data please refer to chapter 6.2. B Figure 3-10:

Flow Cell B A Pipeline with nominal width 50 ... 150 mm A A: High-frequency connections B: Process connection, flanges of different sizes The flow cell consists of a sturdy stainless steel body. The micro-

wave transmitter and receiver are firmly welded to the outside of the pipe. The entire product pipe is PTFE-coated and fulfills the special requirements for use in foodstuffs. There are not objects extending into the pipe (such as measuring sensors). The flow cell can be installed in the pipeline via flange. The flow cell has two HF connections to feed in and output micro-

wave signals. Input and output can be allocated as needed (M-Tx, M-Rx). The microwave signals transmit the product over the entire pipeline cross-section. DynFAS MW 23 Chapter 3 System Description 3.4.3 Container Probe Two different container probe versions are available either with or without flushing device (see Figure 3-11). For technical data please refer to chapter 6.2 Technical Data. Probe with flushing device Probe without flushing device B Figure 3-11:

Container probes A A A: High-frequency connections B: Process connection, flanges of different sizes The container probe has been specially designed for concentration measurements in containers. Both measuring rods are immersed into the product. Microwaves are emitted from one end of the rod and received by the other end of the rod; they are emitted only towards the opposite end of the rod. This direction characteristic of the probe minimizes the interfering influence of metal parts in the vicinity of the probe and allows installation if only little space is available. For example, the concentration of sugar strike can be measured continuously to find the suitable inoculation time. The plastic rods meet the special requirements for application in foodstuffs. 24 DynFAS MW Chapter 3 System Description Two different probe types are available:

The standard type is the container probe without flushing de-

vice

The probe with flushing is employed in processes where incrus-

tations are likely to occur, for example, due to increased depo-

sitions. The flushing device prevents any deposition on the mi-

crowave exit windows. Long travel times are supported by con-

tinuous crystal processes (i.e. VKT). The flow direction of the product being measured should be verti-

cal, as shown in Figure 3-12. This ensures that the product be-

tween the measuring rods is representative, provided it is mixed thoroughly. m m 0 9 1

Product 100 mm Microwave measuring field Plastic rods Pt100 Container wall Figure 3-12:

Probe Pt 100 HF connections Only the probe without flushing is provided with a Pt 100 and is connected to the control unit via 4-wire cable. The wiring diagram for the Pt 100 is described in chapter 4.3.2 Pin Configuration of the Connector Strip. To reduce the danger of incrustation in the imme-

diate vicinity of the measuring rods, the probe with flushing is not provided with a Pt 100. DynFAS MW 25 Chapter 3 System Description Warning, possible property damages!

Do not open the cover screws on the front of the container probes, see Figure 3-13. Probe flange e.g. Probe DN65 / PN6 14 Flow Strmung R-Tx M-Rx M-Tx do not remove!

130 R-Rx PT100 Figure 3-13:

The front of the probe 1 6 0 Probe with Flushing The probe with flushing device has been designed for processes where depositions, for example, due to incrustations are likely to occur on the probe. The flush probe has two flushing channels which keep the plastic rod free from incrustations; this ensures that the microwaves come into direct contact with the product being measured. All parts coming into contact with the product meet the specific re-

quirements for application in foodstuffs. Figure 3-14 shows the probe design. 26 DynFAS MW Chapter 3 System Description Microwave measuring field Plastic rods Rinsing medium 100 mm Container wall m m 0 2 3

Figure 3-14:

Probe with Flushing 4 x HF connections 2 x 3/8 Flushing connections, internal thread The flushing slit width is the same for both probe rods and shown in Figure 3-15. Plastic rods Flushing pipe Flushing slit

~ 1.5 m m Figure 3-15:

Rod head with flushing pipe DynFAS MW 27 Chapter 3 System Description 3.4.4 High-Frequency Cable High-frequency cables (HF cable) are used to transmit microwaves between probe and evaluation electronics. HF cables change their conductivity (for microwaves) relative to the temperature. Therefore, variations in the ambient temperature would create measurement errors. This error is compensated for by enabling the cable compensation. Influences of the ambient temperature on the signal cable are compensated for by means of the reference cable. The reference cable has the same length as the signal cable; during operation, it should be exposed to the same ambient temperature. Therefore, we recommend installing both cable types together in a corrugated tube; this also simplifies installation. The HF cable quad (see Figure 3-16) consists of four individual HF cables of the same length, which each end with one HF plug con-

nector (N-type). Available cable lengths: 2, 4, 6 and 10 m. When connecting the Flow Cell, the reference cable is short-

circuited to the probe side by means of N-connectors (see Figure 3-17). Never bend HF cables! The bending radius should not be less than 100 mm. After installation, fix cables with cable binders. 4 x N-connector 4 x N-

Figure 3-16:

HF-cable quad 0.35 m 18.5 mm Corrugated tube 4 x N-connector Lengths 2, 4, 6 and 10 m 0.35 m 28 DynFAS MW Chapter 3 System Description Sensor side M -R x x R

R R-Tx M

-T x N-connector CC-100 Figure 3-17:

HF-cable quad, at the side of the probe Figure 3-17: The ends of the reference cable R-Rx and R-Tx are short-circuited with an N-connector. For further technical data see chapter 6.3 Technical Data HF-

Cable. DynFAS MW 29 Chapter 3 System Description 3.5 Pipeline Measurement Configuration The control unit is installed in the immediate vicinity of the con-

tainer probe to keep the HF-cable between control unit and probe fairly short. The shorter the cable connection, the better the stabil-

ity of the measurement. The standard length is 4 m and the maxi-

mum length of the HF-cables is 10 m. The flow cell is installed into the existing pipeline system inline or into a bypass. The orientation of the flow cell may either be verti-

cal or horizontal. To rule out sedimentary depositions, vertical in-

stallation in a riser is preferred (see Figure 3-18). The flow cell should be installed fairly close to the sampling loca-

tion to ensure representative sampling for calibration. For possibly required product temperature compensation, a repre-

sentative temperature signal (current signal or Pt 100) has to be connected to the control unit. Control Unit Distance:

typical 4 m Figure 3-18:

Typical measurement configuration on a pipeline HF-cable quad Reference line with N-connector CC-100 Sampling Product flow Orientation:

HF-connections facing down Pipeline inline or in bypass 30 DynFAS MW Chapter 3 System Description 3.6 Container Measurement Configuration The control unit is installed in the immediate vicinity of the probe to keep the HF-cable between control unit and probe fairly short. The shorter the cable connection, the better the stability of the measurement. The standard length is 2 or 4 m and the maximum length of the HF-cables is 10 m. The control unit should be installed fairly close to the sampling location to ensure representative sampling for calibration. A repre-

sentative temperature signal (current signal or Pt 100) should be connected to the control unit for possibly required product tem-

perature compensation. Our example below shows the measurement configuration on a discontinuous evaporation crystallizer. The probe is fixed to the container wall such that both measuring rods are immersed into the product. Figure 3-19:

Typical system configuration on a evaporation crystallizer Distance typical 4 m

(no radiation heat) a a > 60 mm PT-100 HF quad cable Product Microwave measuring field Pt100 Container wall HF connections DynFAS MW 31 Chapter 4 Getting Started Chapter 4. Getting Started 4.1 Transport IMPORTANT Risk of damage!

System parts may get damaged during transportation!

Transport probe and control unit in their original packaging. Pro-

tect parts against shocks. Especially the plastic rods of the con-

tainer probes have to be protected against mechanical impact!

After unpacking, make sure all parts listed on the packing list have been delivered and show no sign of damage; if necessary, clean these parts. If you detect any damage, please notify the forwarder and the manufacturer immediately. The weight of the system components can amount to more than 25 kg depending on the model. You should wear safety shoes. 4.2 Installation 4.2.1 Flow Cell Installation For installation of the flow cell please keep in mind:

The flow cell is installed into the pipeline system. Keep in mind that material sampling should be possible for calibration di-

rectly behind the flow cell.

The flow cell should be installed in a vertical riser, if possible. It has to be ensured that no material depositions occur on the pi-

pe walls and no bubbles are present in the product. For hori-

zontal installation, please observe the correct orientation of the HF-connections (see Figure 4-2).

There should be a straight pipe section of at least 200 mm and equal nominal width before and after the flow cell to ensure a fairly homogeneous flow profile and to rule out possibly occur-

ring microwave reflections in the pipeline. 32 DynFAS MW Chapter 4 Getting Started

No gas bubbles should be present in the product. If gas bub-

bles cannot be ruled out, a pressure of at least 4 bar is re-

quired in the pipeline to minimize the influence of gas bubbles. Please observe the max. permissible working pressure (see chapter 6.2 Technical Data Sensors)

The high-frequency cable should preferably be connected to the flow cell from below to prevent inflowing water from getting to the connecting sockets.

The HF cable should not come into contact with the warm pipe-

lines. Figure 4-1:

Installation in a vertical riser Figure 4-2:

Horizontal installation:

orientation of HF-connections m m 0 0 2

. n m i x R M

) x T

M

Flow cell Orientation:

HF-connections facing down Sampling Product flow Flange 200 ... 250 Nm HF-connections max. 2 Nm Pipeline inline or in bypass x T

M

) x R M

Wrong arrangement !

Correct arrangement !

DynFAS MW 33 Chapter 4 Getting Started 4.2.2 Container Probe Installation For installation, please keep in mind:

Select the installation site such that good mixing and a homo-

geneous product are ensured and no bubbles are present in the probe. A tap should be provided in the direct vicinity to allow representative sampling.

The probe has to be flange-mounted on the container such that the product being measured flows between both measuring rods. That means the fork (both measuring rods) has to be in-

stalled at an angle of 90 to the material flow.

The distance between the measuring rod tips and any metal-

ized walls (heating elements, stirrer, container wall) should be at least 60 mm.

The following installation hole sizes in the fitting flange are required for installation of the probe:

Flange DN 65 / PN 6 others Minimum installation hole size (mm) 100 0.2 102 0.5

For further installation dimensions please refer to chapter 8

(see installation sheets).

Use the respective flat gasket (standard accessory) to compen-

sate for minor surface tolerances in the fitting flange. Installation on Process Containers Figure 3-19 shows the position of the container probe on the con-

tainer. This position is also valid for the container flush probe. The assembly sheet in chapter 8 includes all the information re-

quired for installation. Installation in Pipelines The container probes can be installed in pipelines with a nominal width 200 mm using an adapter flange. Please observe the posi-

tion and orientation of the container probe (see the technical drawings in chapters 8.4.7 and 8.5.6 Installation Situation in Pipe-

lines). 34 DynFAS MW Chapter 4 Getting Started Connection of the flushing pipes The container probe with flushing device consists of two flushing devices with a 3/8 inch inner thread (DIN ISO 228-1). The flushing connections are subsequently sealed to this thread. A sealing to the probe cover is not permitted, for example with silicone. Flush Parameters (only for container flush probe) The degree of deposition or incrustation is essential for the flush parameters, i.e. flush frequency and duration. The flush parame-

ters have to be adapted to the product and the process. The following independent flushing parameters for products and processes have to be observed:

Flush solution Temperature of flush solution Pressure Fittings water, condensation Maximum 120 C 3 bar, max. 8 bar 2 x 3/8 inch female screw thread

(DIN ISO 228-1) 1/2 inch every 2 hours 12 seconds average product temperature, mostly 65 5C Supply pipe Independent flushing parameters product and process, typical starting rates:

Interval Duration Temperature of flush solution For measurements on the C-product the flushing intervals can be considerably reduced, e.g. every 6 hours for 30 seconds. The following is generally valid: the flushing devices can be flushed simultaneously or in shifts. The flushing parameters are valid for every flushing device. Tip The required flush duration has to take into account a possible inertness of the system, e.g. valve openings. The flush supply pipes have to be insulated well against heat to prevent that the flush solution is initially colder. Amount of water The amount of water per flushing connector is approx. 0.8 l/sec at a flushing pressure of 5 bars. DynFAS MW 35 Chapter 4 Getting Started 4.2.3 Installing the Control Unit For installation of the control unit, please keep in mind:

Install the control unit in the vicinity of the microwave probe, keeping in mind the length of the HF cable. HF cables are available in a length of 2, 4, 6 and 10 m; the standard cable length are 2 or 4 m.

Protect the instrument against vibrations.

For instrument installation you should foresee a cutoff device to allow easy and quick disconnection of the device from the power supply.

When installing the control unit on a crystallizer, use a distance rail to minimize thermal radiation and heat conduction. See Figure 4-3.

When the control unit is set-up outdoors, it has to be protected from direct sunshine and rain for example by means of an ade-

quately large protective roof. Figure 4-3:

View from above:

Installation of control unit on a crystallizer Insulation container wall Spacer Control Unit 36 DynFAS MW Chapter 4 Getting Started 4.3 Connecting the Control Unit 4.3.1 Connecting the HF Cable For the connection of the sensor with the control unit, you will need a HF cable quad. Additionally, the flow cell requires an N-

connector. Prerequisite for a proper measurement is the correct installation of cables! Please keep in mind:

IMPORTANT Make sure the cables do not get into contact with hot pipes over the entire length (corrugated tube and single cable section after splitting), e.g. direct contact with the device wall (not insulated). This alone guarantees that all single cables are subject to the sa-

me ambient conditions and that the compensation of the cable drift works properly. Never bend HF cables! The bending radius should not be less than 100 mm. After installation, fix the cables with cable binders to prevent the cable from slipping!

Connecting the Flow Cell The HF-cable quad and the HF-connections on the control unit are labeled. Connect the flow cell to the control unit as shown in Figure 4-4 and make sure that you only connect cables with equal label-

ing. The two connections on the flow cell are not labeled, the allo-

cation of the cable connectors M-Tx and M-Rx is arbitrary. The ca-

ble plugs R-Tx and R-Mx are connector to the N-connector (short-

circuited). DynFAS MW 37 Chapter 4 Getting Started Figure 4-4:

Connection of flow cell version 1 Control Unit, underside M-Rx M-Tx R-Tx R-Rx x R M

x T

M x T

R x R R

Flow cell Bending radius min. 100 mm HF-cable quad

(standard 4 m) Flange 200 ... 250 Nm HF-connections max. 2 Nm x T

M

) x R M

R-Rx R-Tx x R M

) x T

M

Reference line with N-connector Connecting the Container Probes The HF cables and the HF connections on the control unit and on the probe are labeled. Connect the flow cell to the control unit as shown in Figure 4-5, and make sure that you only connect cables with equal labeling. Control Unit, underside M-Rx M-Tx R-Tx R-Rx x R M

x T

M x T

R x R R

Microwave measuring field 0 0 1 M-Tx R-Tx R-Rx M-Rx PT-100 HF quad cable Figure 4-5:

Connection of the container probe to the control unit 38 DynFAS MW Chapter 4 Getting Started IMPORTANT When tightening the 21 mm screw nut, make sure that the con-

nector is not twisted on the cable. If the connector is twisted rela-

tive to the cable, the shielding may get damaged and this could result in mismatching and bad sealing. Hand tighten all screwed connections of the HF cable (2 Nm = 0.2 kg/m)! Before tightening, carefully screw on the cable by hand. Caution! Threaded joint jams easily. Occasionally you should check if the screwed connection is still properly tightened. If the installation is exposed to vibrations, the screwed connection may come loose and this may result in inaccu-

rate measurements or corrosion of the connections. As long as the cables are not connected, the coaxial sockets have to be covered immediately with plastic caps and the cable connec-

tors have to be protected by suitable provisions against moisture and dirt. DynFAS MW 39 Chapter 4 Getting Started 4.3.2 Pin Configuration of the Connector Strip Electrical shock hazard:

Disconnect power to rule out any contact with live parts during installation and when servicing. Turn off power supply before opening the instrument. NEVER work on open and live instruments. Temperature Signal Connection A Pt 100 or a temperature current signal has to be connected to current input 1 or 2 if temperature fluctuations occur in the prod-

uct and if a temperature dependence of the phase or attenuation measurement is likely to occur. The temperature sensor has to measure the material temperature in the vicinity of the microwave probe. When taking the container probe into operation, connect the 4wire cable of the Pt 100 to the connector strip of the control unit as follows:

Figure 4-6:

Pt 100 connection container probe Control Unit Connector strip

(23)

(11) blue blue white white PT-100 sensor in the container probe

( ) Terminal no. 40 DynFAS MW Chapter 4 Getting Started Other Connections

Connect all desired input and output signals to the terminal strip as shown below. Use the M feed-through to maintain the degree of protection.

Check if the voltage indicated on the type plate matches your local supply voltage.

Connect the line cable to the terminals 3(L1), 2(N) and 1(PE).

Check if the test switch (mains interruption) is in position on

(see Figure 5-1).

Close the instrument housing and turn on the power supply. Attention! Possible danger, damage to property! Concerns the sys-

tem type CH-200-024 Control Unit High Dynamic 24 V DC (Id.-No. 54878-02):

When connecting the 24 V DC auxiliary power, the + and Poles should be connected correctly. There is no reverse voltage protec-

tion!

The line cross-section for the power supply must be at least 1.0 mm2. On the connector strip of the control unit you find the following connections:

or / bzw.

Figure 4-7:

DynFAS MW wiring diagram DynFAS MW 41 Chapter 4 Getting Started Power supply: Terminals 3 (L1, +), 2 (N, -) and 1 (PE, ) For CS-100, depending on instrument version, see type label on the outer wall of the housing. 1.) 90 V - 265 V AC, 45 - 65 Hz 2.) 24 V DC: 18 36 V 24 V AC: -20%, +5%, 40 440 Hz For CH-200, depending on instrument version, see type label on the outer wall of the housing. 1.) 90 V - 265 V AC, 45 - 65 Hz 2.) 24 V DC: 18 36 V, no reverse voltage protection Current input no. 1 (terminals 20+ and 8-), insulated Input as 0/4 - 20 mA signal. e.g. for temperature compensation or reference signal recording. Current input no. 2 (terminals 22+ and 10-), not insulated Input as 0/4 - 20 mA signal. e.g. for temperature compensation or reference signal recording. Current output no. 1 (terminals 27+ and 15-), insulated Output as 4 - 20 mA signal. Output options: concentrations (1/2), current inputs signals (1 / 2) and Pt 100 signal Current output no. 2 (terminals 19+ and 7-), insulated Output as 0/4 - 20 mA signal. Output options: concentrations 1 and 2, current input signals 1 and 2 and Pt 100 signal Pt 100 (terminals 23+ and 11-) Connection for temperature measurement. Digital input 1: DI1 (terminals 24+ and 12-) Configuration options:

no function

measurement: start (closed) and stop (open) Digital input 2: DI2 (terminals 25+ and 13-) Configuration options:

no function

average value: hold (closed) and continue averaging (open)

product selection: product 1 (open) and product 2 (closed) 42 DynFAS MW Chapter 4 Getting Started Digital input 3: DI3 (terminals 26+ and 14-) Configuration options:

no function

start sampling, open: no action, closed: unique measurement starts

product selection Relay 1: (terminals 4, 5 and 6) Changeover contacts (SPDT), insulated, configuration option:

no function

error message

stop measurement

no product Relay 2: (terminals 16, 17 and 18) limit value min. and max. Changeover contacts (SPDT), insulated, configuration option:

no function

error message

stop measurement

no product RS485 interface (terminals 21 (RS1) and 9 (RS2)) limit value min. and max. Serial data interface for output of live data (all measuring data for every sweep, measuring cycle) the setup protocol and data log. Data format: 38400 baud, 8 data bits, 1 stop bit, no parity, no handshake. RS232 interface (on instrument bottom) 9-pole SubD-connector. Serial data interface for output of live data

(all measuring data for every sweep, measuring cycle) the setup protocol and data log. Data format: 38400 baud (Data transfer rate ), 8 data bits, 1 stop bit, no parity, no handshake. DynFAS MW 43 Chapter 4 Getting Started 4.3.3 Digital Outputs, Relays The status of the measurement is output via two relays:

Error

Alarm (alarm min. and max.)

No product Under menu item Plausibility, you may enter a min. attenuation for pause detection (e.g. for process pause, no product pre-

sent); if this value is not reached, no product is signaled via a relay and the current output drops to 0 or 4 mA. A typical application is pause detection between the discontinu-

ous evaporation crystal processes.

Measurement stopped The respective switching status is also signaled via LEDs on the front panel (LEDs: signal 1 and 2). Relay no. Error, alarm, no product, measurement stopped, currentless status 1 2 4 5 6 16 17 18 com com Normal 4 5 6 16 17 18 com com The relays with changeover contacts can either be operated as make contact, terminals 4 & 5 (open at error, alarm ...) or as break contact, terminals 5 & 6 (closed at error, alarm ...). 44 DynFAS MW Chapter 5 Service Instructions Chapter 5. Service Instructions 5.1 General Information The control unit has no wearing parts or components requiring any special maintenance. A malfunction of the measuring system is not always due to a de-

fect in the instrument. Often the error is caused by incorrect op-

eration, wrong installation, or irregularities in the product being measured. If a malfunction occurs, anyway, the measuring system helps you to identify and eliminate errors by displaying error messages on the LCD, indicating operator errors and defects of the electronics. Usually, faulty modules of the control unit cannot be repaired but have to be replaced. The microwave module is fixed with screws to a shielding cover and must not be opened. 5.2 Wearing Parts The control unit consists of no wearing parts and components that need special attention. The plastic rods of the Probes and the PTFE lining of the Flow Cell can eventually experience abrasion depending on the material be-

ing measured. A lower to middle abrasion influences inconsiderably the measurement or is compensated by calibration. Therefore, you should check the wearing parts approximately every 2 years. The plastic rods of the Probe and the lining of the Flow Cell can be exchanged if abrasion is heavy. During excessive wear, the plastic rods of the Probe and the lining of the Flow Cells can be ex-

changed. These Probes and the Flow cells have to be sent back to the company. An on-site exchange is not possible. 5.3 Instrument Cleaning Clean all system components using a moistened cloth. Do not use any chemical cleaning agent. Parts coming into contact with the product (during regular operation) can be cleaned with hot water, taking into account the temperature limits (see chapter 6.2 Technical Data Sensors). DynFAS MW 45 Chapter 5 Service Instructions 5.4 Battery If the measuring system DynFAS MW is without power supply

(power failure or disconnected from mains), the system clock is supplied with power by the Lithium battery on the CPU. The in-

strument works correctly even with empty battery, only measured data which are output via one of the serial interfaces may become useless as a result of the faulty date and time information. The service life of the battery, even under continuous load, is at least 8 years. To replace the battery, you have to disconnect the instrument from mains. Battery type: 3 Volt Lithium cell (round cell battery), type CR2032. 5.5 Fuse Replacement The mains fuse of the DynFAS MW is located in the wall housing. Replace the fuses only if the instrument is disconnected from mains. Be sure that the new fuses match the rating specified. Use only fuses with correct rating:

For CS-100:

Instrument version with 90 ... 265 V AC: 2.0 A slow-blow Instrument version with 24 V AC/DC: 2.0 A slow-blow For CH-200:

Instrument version with 90 ... 265 V AC: 2.0 A slow-blow Instrument version with 24 V DC: 6.3 A slow-blow Spare fuses must match the rating specified by the device manu-

facturer. Short-circuiting or manipulation is not permitted. Test switch Fuses Line connector Feed-through for line connector Netzteil I 0 Protective cover Motherboard EEprom

(can be pulled off) Terminal strip

(can be pulled off) Battery Figure 5-1:

Look inside the instrument CS-100 46 DynFAS MW Chapter 6 Technical Data Chapter 6. Technical Data General Specifications Method Microwave transmission measurement Working frequency 2.4 2.5 GHz (ISM band), depending on local regulations Transmission power CS-100: < 0.1 mW (< -10 dBm) CH-200: < 10 mW (< 10 dBm) All coaxial line power Applications Concentration measurement in containers and pipes 6.1 Control Unit Control unit Housing Wall housing made of stainless steel, material 1.4571 (~316+Ti), see dimensional drawing in chapter 8. CS-100: HxWxD: 300 x 323 x 140 mm CH-200: HxWxD: 400 x 338 x 170 mm Protection type IP 65 Weight Operating temperature Storage temperature Achievable accuracy Display Keyboard Power supply CS-100: approx. 6.5 kg CH-200: approx. 8.0 kg

-20 ... +60C ( 253 ...333 K ), Humidity 0 90% relatively, no condensation

-20 ... +80C ( 253 ...353 K ), Humidity 0 90% relatively, no condensation 0.2 weight % (standard deviation) depending on product and sensor Dot matrix LC display, 114 mm x 64 mm, 240 x 128 pixels, with back-lighting, automatic contrast setting Freely accessible foil keypad, light-stable and weatherproof: alphanumeric keyboard and four softkeys (software-assigned buttons) For CS-100 depending on instrument version:

1.) 90 ... 265 V AC, 45 ... 65 Hz or 2.) 24 V DC: 18 ... 36 V 24 V AC: -20%, +5%, 40 ... 440 Hz For CH-200 depending on instrument version:

1.) 90 ... 265 V AC, 45 ... 65 Hz or 2.) 24 V DC: 18 ... 36 V, no reverse voltage pro-

tection DynFAS MW 47 Chapter 6 Technical Data Power consumption For CS-100:

max. 30 VA (AC/DC), depending on configuration For CH-200:

max. (48/60) VA (AC/DC), depending on configu-

ration Fuses For CS-100:

2 x 2.0 A / slow-blow For CH-200:

2 x 2.0 A / slow-blow for 90 265 V AC or 2 x 6.3 A / slow-blow for 24 V DC Battery type 3 V Lithium button cell, type CR2032 Measured value e.g. concentration, dry content Inputs and Outputs Cable cross-section Cable feed-through Sensor connection HF-cable Current input Current output min. 1.0 mm (mains supply) 2 x M20x1.5 for cable 5...14 mm (depending on application) 4 x M16x1.5 for cable 5 ...8 mm

(depending on application) Inputs and outputs for signal and reference channel, 50 N-socket Cable lengths: 2, 4, 6 and 10 m; 50 ;

both sides with 4 N connectors 2 x current input 0/4 ...20 mA, ohmic resistance 50 , 1x insulated, 1x instrument ground e.g. for temperature compensation Current output 1: 4...20 mA, ohmic resistance max. 800 , insulated current output 2: 0/4...20 mA, ohmic resistance max. 800 , insulated e.g. for measured value or temperature output Pt 100 connection Measuring range: -50 ... +200C (223 ... 473 K);

measurement tolerance: < 0.4C 48 DynFAS MW Chapter 6 Technical Data Digital input Relay outputs 3 x digital inputs (DI1..3), for floating connectors Configuration options:

DI1: none, measurement start/stop DI2: none, measurement hold, product selection DI3: none, sampling, product selection Function description:

1. Measurement (Start/Stop) open: measurement stopped closed: measurement started or measurement running 2. Hold measurement open: measurement running closed: measurement stopped, i.e. average values and current output are held 3. Product selection open: product 1 (P1) closed: P2;

with two DIs: DI2 open & DI3 open: P1, DI2 closed & DI3 open: P2, DI2 open & DI3 closed:

P3, DI2 closed &DI3 closed: P4 4. Start sampling open: no actions closed: single measurement starts 2 x relays, insulated Configuration options:

- Collective failure message

- Stop measurement

- Limit value (alarm min. and max.)

- No product max. 400VA max. 90W Load capacity:

AC:

DC:

AC / DC: max. 250V, max. 2A, non-inductive 150V: voltage must be grounded The cable and insulation that are to be connected to these cables must correspond to a mains con-

nection. Restrictions for 24 V AC/DC mains supply, if the ground conductor is not connected to terminal 1

(PE):

AC: max. 50 V DC: max. 70 V Serial interfaces RS 232 on the underside of the instrument, RS 485 through terminal block Data type: 38400 baud, no handshake, 8 data bits, 1 stop bit, no parity DynFAS MW 49 Chapter 6 Technical Data 6.2 Technical Data Sensors Flow Cells Application Material Process coupling Process pressure Microwave flow cell with various nominal widths and flanges for measurement on pipelines Stainless steel, PTFE lining Flange according to DIN EN 1092 Type 05 and ASA Up to 20 bar (relative), depending on nominal width and flange type, see table below Temperature range Product temperature: +10 ... +130C (283 403 K) Ambient temperature: -20 ... +60C (253 333 K) Storage temperature: +10 ... +80C (283 353 K) Connections Versions Dimensions 2 x HF connections: N-socket, 50 for HF-cable with max. 10 m length Nominal pipe widths from 50 ... 150 mm See dimensional drawings in chapter 8 Overview Flow Cells Designation ID-No. Nominal Flange FC-050-016 FC-065-040 FC-080-016 FC-100-016 FC-150-016 FC-020-150 FC-025-300 FC-030-150 FC-040-150 FC-060-150 width

[mm]

50 65 80 100 150 50 65 80 100 150 54943 54944 54945 54946 54941 54947 54948 54949 54950 54951 DN 50 / PN 16 DN 65 / PN 40 DN 80 / PN 16 DN 100 / PN 16 DN 150 / PN 16 ASA 2 / 150 PSI ASA 2.5 / 300 PSI ASA 3 / 150 PSI ASA 4 / 150 PSI ASA 6 / 150 PSI 16 20 16 16 16 16 20 16 16 16 Pressure

[bar]

50 DynFAS MW Chapter 6 Technical Data Probes Application Material Process coupling Probes with and without flushing device for concentration measurement in process containers and pipelines with nominal width 200 mm. Plastic rod, stainless steel PT100 connection cable: Silicon / Teflon Flange according to DIN EN 1092 Type 05 DN65 / PN6, DN 80, 100, 150 / PN16;

ASA flange 2.5, 3 / 150 PSI Process pressure Up to 16 bar (relative), depending on model Temperature range Product temperature: +10 ... +120C (283 393 K) Ambient temperature: -20 ... +60C (253 333 K) Storage temperature: +10 ... +80C (283 353 K) Connections 4 x HF connections: N-socket, 50 for HF-cable with max. 10 m length Dimensions See dimensional drawings in chapter 8 Accessory sealing washer Material Thickness Klingersil C-4400 3 mm Overview Probes Designation ID-No. Flange Pressure

[bar]

P-065-006 P-080-016 P-100-016 P-150-016 P-025-150 P-030-150 PF-065-006 PF-080-016 PF-100-016 PF-150-016 PF-025-150 54939-01 54939-02 54939-03 54939-04 54939-05 54939-09 54940-01 54940-02 54940-03 54940-04 54940-05 DN 65 / PN 6 DN 80 / PN 16 DN 100 / PN 16 DN 150 / PN 16 ASA 2.5 / 150 PSI ASA 3 / 150 PSI DN 65 / PN 6 DN 80 / PN 16 DN 100 / PN 16 DN 150 / PN 16 ASA 2.5 / 150 PSI 6 16 16 16 16 16 6 16 16 16 16 DynFAS MW 51 Chapter 6 Technical Data 6.3 Technical Data HF-Cable HF-Cable Quad Material Corrugated tube: Polyamide (PA6) Cable sheath: Polyethylene (PE) Protection type IP 66 Temperature Operating temperature: -30 ... +70C (243 343 K) Installation temperature: -20 ... +70C (253 343 K) Summary HF-Cable Quad, Cable lengths Length [m]

2.0 4.0 6.0 10.0 Id No. 54856 54857 54858 54859 52 DynFAS MW Chapter 6 Technical Data 6.4 Format of Serial Data Output RS 232 and RS 485 Header DateTimeFlagsStatusProductAttPhiR2TintIN1IN2Pt 100CCmC2C2m Following lines 01.01.200500:00:000000010.435.300.070.00.00.00.075.3675.000.000.00 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 4 5 6 7 8 9 10 11 12 13 14 15 Column no. Description 1 2 3 Date and time Flags (for test purposes) Status: Information on quality of last measurement Product number Attenuation [dB]

Phase [/GHz]

Statistical spread of phase regression Instrument temperature [temperature unit]

Current input 1 [unit of current input]

Current input 2 [unit of current input]

Pt 100 temperature [temperature unit]

Format DD.MM.YYHH:MM:SS 4 digits, HEX 0 : measurement OK

< 0 : error X (1 to 4) X.XX X.XX X.XX X.X X.X X.X X.X Concentration 1 live Concentration 1 averaged Concentration 2 live Concentration 2 averaged

[] by selection of unit g/cm3 X.XX [X.XXXX]

X.XX [X.XXXX]

X.XX [X.XXXX]

X.XX [X.XXXX]

Special characters Tabulation Carriage return + Line feed Blank character DynFAS MW 53 Chapter 7 Certificates Chapter 7. Certificates 7.1 EC Declaration of Conformity DynFAS MW 55 Chapter 7 Certificates 56 DynFAS MW Chapter 7 Certificates 7.2 Frequency Approval DynFAS MW 57 Chapter 7 Certificates 58 DynFAS MW Chapter 7 Certificates DynFAS MW 59 Chapter 7 Certificates 60 DynFAS MW Chapter 7 Certificates DynFAS MW 61 Chapter 7 Certificates 62 DynFAS MW Chapter 8 Technical Drawings Chapter 8. Technical Drawings 8.1 Dimensional Drawing of Control Unit Housing 8.1.1 Control Unit Standard CS-100 DynFAS MW 63 Chapter 8 Technical Drawings 8.1.2 Control Unit High Dynamic CH-200 64 DynFAS MW Chapter 8 Technical Drawings 8.2 Electrical Wiring Diagram Line in for CS-100:

1. / 2. depending on instrument version 1. AC 90-265V, 45-65 Hz 2. DC 24 V (18-36 V) or AC 24 V -20% / +5%, 40-440 Hz ________________________________ Line in for CH-200:

1. / 2. depending on instrument version 1. AC 90-265V, 45-65 Hz 2. DC 24 V (18-36 V), no reverse voltage protection DynFAS MW 65 Chapter 8 Technical Drawings 8.3 Dimensional Drawings Flow Cells 8.3.1 Type FC-050-016 66 DynFAS MW Chapter 8 Technical Drawings 8.3.2 Type FC-065-040 DynFAS MW 67 Chapter 8 Technical Drawings 8.3.3 Type FC-080-016 68 DynFAS MW Chapter 8 Technical Drawings 8.3.4 Type FC-100-016 DynFAS MW 69 Chapter 8 Technical Drawings 8.3.5 Type FC-150-016 70 DynFAS MW Chapter 8 Technical Drawings 8.3.6 Type FC-020-150 DynFAS MW 71 Chapter 8 Technical Drawings 8.3.7 Type FC-025-300 72 DynFAS MW Chapter 8 Technical Drawings 8.3.8 Type FC-030-150 DynFAS MW 73 Chapter 8 Technical Drawings 8.3.9 Type FC-040-150 74 DynFAS MW Chapter 8 Technical Drawings 8.3.10 Type FC-060-150 DynFAS MW 75 Chapter 8 Technical Drawings 8.4 Dimensional Drawings Probes 8.4.1 Type P-065-006 76 DynFAS MW Chapter 8 Technical Drawings 8.4.2 Type P-080-016 DynFAS MW 77 Chapter 8 Technical Drawings 8.4.3 Type P-100-016 78 DynFAS MW Chapter 8 Technical Drawings 8.4.4 Type P-150-016 DynFAS MW 79 Chapter 8 Technical Drawings 8.4.5 Type P-025-150 80 DynFAS MW Chapter 8 Technical Drawings 8.4.6 Type P-030-150 ll DynFAS MW 81 Chapter 8 Technical Drawings 8.4.7 Installation Situation in Pipelines 82 DynFAS MW Chapter 8 Technical Drawings 8.5 Dimensional Drawings Flush Probes 8.5.1 Type PF-065-006 DynFAS MW 83 Chapter 8 Technical Drawings 8.5.2 Type PF-080-016 84 DynFAS MW Chapter 8 Technical Drawings 8.5.3 Type PF-100-016 DynFAS MW 85 Chapter 8 Technical Drawings 8.5.4 Type PF-150-016 86 DynFAS MW Chapter 8 Technical Drawings 8.5.5 Type PF-025-150 DynFAS MW 87 Chapter 8 Technical Drawings 8.5.6 Installation Situation in Pipelines 88 DynFAS MW Chapter 8 Technical Drawings 8.6 Installation Sheets for DynFAS MW (Probe) DynFAS MW with Probe

- Installation In Crystallizer -

top view into the crystallizer evaluation unit botten side 90 - 265 V AC or 24 V AC/DC

(24 V DC) output 0/4 - 20 mA 190 PT100 microwave measuring field 0 0 1 60 M-Tx R-Tx R-Rx M-Rx 0 6 1 container wall sealing probe flange DN65 / PN6 insulation installation position 14 Flow Strmung R-Tx do not remove!

M-Rx M-Tx R-Tx R-Rx x R M

x T

M x T

R x R R

PT100 HF cable quad Control Unit

(...) for CH-200 300

(318) 0 2 2

) 0 2 3

M-Rx M-Tx 130 R-Rx PT100 heating 1 6 0 current stream fitting flange 130 / 4 x M12 100 0.2 60 area without metalic installations DynFAS MW 89 Chapter 8 Technical Drawings DynFAS MW with Probe

- Installation In Crystallizer -

top view into the crystallizer evaluation unit botten side 90 - 265 V AC or 24 V AC/DC

(24 V DC) output 0/4 - 20 mA container wall 190 microwave measuring field PT100 0 0 1 60 M-Tx R-Tx R-Rx M-Rx B probe flange DN80, 100, 150 / PN16 sealing M-Rx M-Tx R-Tx R-Rx x R M

x T

M x T

R x R R

PT100 HF cable quad Control Unit

(...) for CH-200 300

(318) DN A 80 100 150 B C S 160 200 18 M16 180 220 18 M16 240 285 22 M20 insulation 0 2 2

) 0 2 3

R-Tx do not remove!

installation position C M-Rx M-Tx A R-Rx B PT100 current stream fitting flange A / 8 x S 102 0,5 heating 60 area without metalic installations 90 DynFAS MW Chapter 8 Technical Drawings 8.7 Installation Sheets for DynFAS MW (Flush Probe) DynFAS MW with Probe with Flushing

- Installation In Crystallizer -

top view into the crystallizer 320 microwave measuring field evaluation unit botten side 90 - 265 V AC or 24 V AC/DC

(24 V DC) output 0/4 - 20 mA M-Rx M-Tx R-Tx R-Rx x R M

x T

M x T

R x R R

0 0 1 160 M-Tx R-Tx R-Rx M-Rx 0 6 1 container wall sealing HF cable quad Control Unit

(...) for CH-200 300

(318) probe flange DN65 / PN6 installation position 14 Flow Strmung R-Tx insulation do not remove!

0 2 2

) 0 2 3

M-Rx M-Tx 5 5 130 R-Rx flushing connection:

internal thread 2 x G3/8

(DIN ISO 228-1) heating 1 6 0 fitting flange 130 / 4 x M12 100 0,2 current stream 60 area without metalic installations DynFAS MW 91 Chapter 8 Technical Drawings 90 - 265 V AC or 24 V AC/DC

(24 V DC) output 0/4 - 20 mA M-Rx M-Tx R-Tx R-Rx x R M

x T

M x T

R x R R

HF cable quad Control Unit

(...) for CH-200 300

(318) 0 2 2

) 0 2 3

DynFAS MW with Probe with Flushing

- Installation In Crystallizer -

top view into the crystallizer container wall evaluation unit botten side 0 0 1 160 M-Tx R-Tx R-Rx M-Rx B probe flange DN80, 100, 150 / PN16 DN A 80 100 150 B C S 160 200 18 M16 180 220 18 M16 240 285 22 M20 sealing insulation microwave measuring field 320 installation position C M-Rx A R-Rx R-Tx M-Tx 5 5 do not remove!

B heating flushing connection:

internal thread 2 x G3/8

(DIN ISO 228-1) current stream 60 area without metalic installations fitting flange A / 8 x S 102 0,5 92 DynFAS MW Index A accuracy 47 adapter flange 34 B Battery 46 bending radius 28 C Calculation of Measured Values 17 CE symbol 13 Certificates 55 Components 19 Connecting the Container Probes 38 Connecting the Flow Cell 37 Container Probe 24 Container Probe Installation 34 Control unit Housing 63 Control Units 20 cooling crystallizers 18 D Data format RS232 53 Data format RS485 53 Data transfer rate 43 Digital Outputs 44 Dimensional Drawings Flow Cells 66 Dimensional Drawings Flush Probes 83 Dimensional Drawings Probes 76 distance rail 36 E EC Declaration of Conformity 55 Electrical Wiring Diagram 65 F Factory setting 15 fitting flange 34 Flow Cell 23 Flow Cell Installation 32 Flush Parameters 35 flush probe 26 DynFAS MW foodstuffs 24 Frequency Approval 13, 57 Fuse Replacement 46 G gas bubbles 14, 33 H High-Frequency Cable 28 I Installation in Pipelines 34 Installation Sheets 89 Installation Situation in Pipelines 82, 88 Instrument Cleaning 45 L LEDs 22 M Measurement Configuration 30, 31 Microwaves 15 O Overview Flow Cells 50 Overview Probes 51 P Principle of Measurement 16 Pt 100 connection 40 R Reference temperature 18 Relays 44 riser 32 RS232 interface 43 Index 93 Index S safety instructions 7 salt content 14 Softkeys 15 symbols 7 T Technical Data 47 Technical Data HF-Cable 52 Technical Data Sensors 50 Technical Drawings 63 Temperature Compensation 18 Transmission power 47 Transport 32 W Wearing Parts 45 94 DynFAS MW Notes DynFAS MW 95 Notes 96 DynFAS MW Concentration Meters DynFAS MW Software Manual User's Guide Id. Nr. 54877BA2 Rev. No.: 00 01.07.2009 The units supplied should not be repaired by anyone other than BMA Schaltanlagen Service engineers or technicians authorized by BMA Schaltanlagen. In case of operation trouble, please address to our central service department. The complete users guide consists of two manuals, the hardware description and the software description. The hardware manual comprises:

mechanical components

installation

electrical installation

radiation protection guidelines

technical data

electrical and mechanical drawings The software manual comprises:

operation of the evaluation unit

parameter description

basic setting

calibration

error messages The present manual is the software description. Subject to changes without prior notice. BMA Schaltanlagen GmbH Am Alten Bahnhof 5 D-38122 Braunschweig Tel. +49 531 804 261 Fax +49 531 804 269 schaltanlagen@bma-de.com www.bma-worldwide.com DynFAS MW Table of Contents Chapter 1. Communication with DynFAS MW 1.1 Brief Instructions 1.2 System Configuration 1.3 System Calibration Chapter 2. Software Functions 2.1 Information on Menu Structure 2.2 Menu Structure 2.2.1 Start Menu 2.2.2 Diagnostic 2.2.3 Setup 2.2.4 Access Level 2.2.5 Language 2.2.6 Configuration 2.2.7 General Data 2.2.8 Measurement 2.2.9 Plausibility 2.2.10 Phase Measurement 2.2.11 Pause Detection 2.2.12 Calibration 2.2.13 System Adjust 2.2.14 Calibrate Concentration 2.2.15 Sample No. 2.2.16 Sample Data (expanded) 2.2.17 Advanced Settings 2.2.18 Calibr. manual 2.2.19 Input / Output 2.2.20 Current output 2.2.21 Current Output 1 2.2.22 Current Output 2 2.2.23 Current input 2.2.24 Current In 1 2.2.25 Current In 2 2.2.26 Pt 100 2.2.27 Digital Output 2.2.28 Digital Input 2.2.29 Service 2.3 Trend Display Chapter 3. Configuration 3.1 Configuration Setup 3.1.1 General Data 3.1.2 Measurement 3.1.3 Plausibility 3.1.4 Microwave 3.1.5 Marker 3.1.6 Units 3.2 Start Calibration Coefficients Page 9 10 10 10 11 11 12 14 14 16 17 17 18 19 19 20 21 22 24 24 25 26 27 27 28 28 29 29 30 30 30 30 31 31 31 32 34 35 35 35 36 36 36 37 37 39 DynFAS MW 41 41 43 44 44 46 47 49 50 52 52 55 59 61 64 66 67 68 69 69 70 71 73 74 75 75 76 78 78 79 80 80 81 82 83 85 85 85 85 86 Chapter 4. Calibration 4.1 System Calibration 4.2 Start-up of CH-200 4.3 Start Calibration 4.3.1 First Process Run 4.3.2 Sampling 4.3.3 Entering the Lab Values 4.3.4 Automatic Calibration 4.3.5 Automatic Calibration with Temperature Compensation 4.4.1 Manual Calibration with one Concentration 4.4.2 Calibration with Two Concentrations 4.4.3 Calibration with Split Value 4.4.4 Calibration with Temperature Compensation 4.4 Manual Calibration 4.5 Adjusting the Calibration 4.6 Output of the start-up protocol Chapter 5. Password 5.1 Forgot password Chapter 6. Inputs / Outputs 6.1 Current Outputs 6.2 Current Inputs 6.1.1 Current Output Setup 6.1.2 Test and Adjustment 6.1.3 Error Current 6.1.4 Current Output 2 6.2.1 Enabling the Current Input 6.2.2 Range Setting and Adjustment 6.3.1 Pt 100 Enabling 6.3.2 Pt 100 Calibration 6.4.1 Digital Output Assignment 6.5.1 External Product Selection 6.4 Digital Output 6.5 Digital Input 6.3 Pt 100 Chapter 7. Factory Settings Chapter 8. Error Lists 8.1 Error Lists 8.1.1 Hardware Error 8.1.2 Input Error 8.1.3 Measurement Error and Error Prompts DynFAS MW Chapter 9. Calibration Data Sheet 9.1 Configuration 9.1.1 General Data 9.1.2 Measurement 9.1.3 Plausibility 9.1.4 Microwave 9.2 Product 9.3 Inputs/Outputs 9.3.1 Current Output 9.3.2 Current Input 9.3.3 Pt 100 Input 9.3.4 Digital Output 9.3.5 Digital Input 9.4 Calibration Data 9.4.1 Calibration Coefficients 9.4.2 Typical Calibration Coefficients 9.5 Start-up protocol printout 9.5.1 Examples of a start-up protocol 9.6 Sample Table 87 87 87 87 87 87 87 88 88 88 88 88 89 89 89 89 90 93 98 DynFAS MW Chapter 1 Communication with DynFAS MW Safety Summary GENERAL WARNINGS Parameter settings No changes should be made in the parameter set-

tings without exact knowledge of the instruction manual with all instructions and detailed knowl-

edge about the properties of a connected control unit and the possible influences to the operation process being controlled. DynFAS MW 7 Chapter 1 Communication with DynFAS MW Chapter 1. Communication with DynFAS MW The communication with DynFAS MW is carried out via 4 softkey buttons. The function of the individual buttons changes relative to the position in the menu. Values and texts are entered via an alphanumeric keyboard. The instru-

ment status is indicated by 5 LEDs. Softkey buttons LEDs LCD display Lock Numerical keypad RS232 connection HF connections for signal cable reference cable and cable feed-through 9 DynFAS MW Chapter 1 Communication with DynFAS MW 1.1 Brief Instructions Provided that DynFAS MW is installed correctly, after power on of the device the main menu ap-

pears automatically. To get correct measurement values, the instrument has to be configured and calibrated before running the first measurement. Go to the Profi mode. We recommend that you use these brief instructions only if you have already performed a process measurement with the same product and you are familiar with the Phi/att ratio. 1.2 System Configuration

Select | Setup | Configuration | General Data

Enter the general data (date, time, tag)

Push the Home button to return to the Configuration menu and select | Measurement |

Enter the system parameters (measurement mode, start mode, averaging, units, ...)

Push the Home button to return to the Configuration menu

Select | Plausibility |

Enter: 1. Process limits; 2. Phase measurement: Sigma max. = 100, Phi/att ratio = known value, Auto set = OFF; 3. Disable pause detection

Push the Home button to return to the Configuration menu

Select | Microwave |

Enter the cable length (reference cable length, signal cable length)

Push the Home button to return to the Setup menu

Select | Input/Output |

Enter the values for current output, current input, Pt100, digital out-/input

Push the Home button to return to the Setup menu. 1.3 System Calibration

Power on the instrument at least 45 minutes prior to system calibration.

On the main menu, select | Setup |Calibration | System Adjust | Adjust |

Start the adjustment only if you are sure that the transducer is sufficiently covered by the prod-

uct. The typical standard coefficients for your application have been set up by the manufacturer. A sample has to be taken during system calibration. The lab value of the sample is needed for calculation of the offset. Calculation: Analysis value Display = Offset.

Upon completion of the system calibration, push the Home button three times to return to the main menu.

Push the RUN softkey to start the measurement. The live display appears.

Push ESC to get to the main display and enter the offset value via | Setup | Calibration | Cali-

brate Conc | Adjust | Offset |.

Enter offset value.

Push the Home button 4 times to return to the main menu.

Select | Live display |

If the product has not changed, the reading value corresponds to the laboratory value. 10 DynFAS MW Chapter 2 Software Functions Chapter 2. Software Functions 2.1 Information on Menu Structure The menu structure on the following pages provides an over-

view of all functions of the DynFAS MW. Using the page numbers indicated you can look up the function of the de-

picted window. Depending on the access level, some menu items are hidden. You have to enter an editable password to change from the level Read only to Basic or to Profi. The Service level is not accessible due to licensing regulations. DynFAS MW 11 Chapter 2 Software Functions 2.2 Menu Structure 1 | - | Live Display | 07.05 13:25 Concentration av. 65.50 %

Conc av. Conc act. 64.35%

ESC SAMPLE .... ZOOM Live Display Diagnostic Setup Access Level Language Page 14 Page 14 Diagnostic Datalog Errorlog Info Print Setup Setup See next page Access Level Read only Basic Profi Service Language English German French Page 17 Page 17 12 DynFAS MW Chapter 2 Software Functions Setup Configuration Calibration Input / Output Service Product Change password Page 16 Current Output Current Out 1 2 Page 29 Page 24 System Adjust Configuration General Data Measurement Plausibility Microwave Markers Units Page 18 Adjust Num. Sweeps Ref. values Chart Phi Chart Attenuation Page 24 Calibration System Adjust Calibrate Conc Advanced Current Out 1 Assignment Upper value Lower value Test/Adjust Error current Page 29 Current Input Current Out 2 Current Input 1 2 Page 30 Page 30 Pt100 Enabled Adjust Pt 100 live Digital Output Relay 1 Relay 2 Test Page 31 Digital Input Status DI 1 function DI 2 function DI 3 function Page 31 Assignment Upper value Lower value Range Test/Adjust Error current Page 29 Current Input 1 Enabled Adjust Live current Current In 2 Enabled Adjust Live current Page 30 Page 30 Page 25 Calibrate Conc Sampling Calibr. autom. Calibr. manual Tuning View Advanced Tara values Num Cal. Sweeps Process Type Split Value Page 27 Page 28 Calibr. manual Cal. Order Cal. Base Coefficients Compensation Start Calibr. Live Display Diagnostic Setup Access Level Language Input / Output Current output Current input Pt100 Digital output Digital input Page 28 DynFAS MW General Data Date Time Tag Page 19 Measurement Meas. Mode Start Mode Averaging Reset averaging Page 19 Plausibility Process limits Phase Measure Pause Detection Phase Measure Sigma max. Phi/att ratio Auto set Sample No Page 20 Page 21 Next sample Active Measured value Lab Value Advanced Page 26 Advanced Current Input 1 Current Input 2 Pt 100 PHI (m) Attenuation Page 27 13 Chapter 2 Software Functions 2.2.1 Start Menu 1 | - | Control Unit | 07.05 13:25 Live Display Diagnostic Setup Access Level Language RUN 2.2.2 Diagnostic LIVE DISPLAY:

Shows the live display. DIAGNOSTIC:

This menu item contains the submenu items data logger, error log and further instrument information. SETUP:

All necessary inputs for operation of the measuring system can be entered here. ACCESS LEVEL:

Areas protected by passwords can be enabled. LANGUAGE:

Select the dialog language. Datalog Errorlog Info Print Setup 1 | - | Diagnostic | 07.05 13:25 Datalog:

The data log records the data corresponding to the content of the serial data output RS 232 and RS 485 (see hardware manual, chapter 6.4). All data per measurement values (sweep) are averaged over the measuring time (see below) and stored. This time inter-

val results from the selected logging period. The content of the log file can be accessed via the Live Display graphically, see chapter 2.3 Trend Display. Output as a text-file is also possible by using RS 232 and RS 485, or the Memory Tool in-

stead (optional accessory). Log type Log time Restart Log Disable single continuous stop at error logging period 15 minutes to 3 days Clears the datalog and starts with the above setting Averaging time Obtained from log time Print log Printout of table, output via RS 232 and RS 485, format see hardware manual, chapter 6.4 14 DynFAS MW Chapter 2 Software Functions Change datalog settings:

If you change the logtype from any to single the datalog will be cleared and you start again with the current set-

ting. If you change all other logtypes and log times, the datalog will not be cleared and you continue with the new settings. Stopped measurement:

If the measurement is stopped for a time during the data log, then the measurement pause is interpreted as log time during the data logging single. For all other log types, the measuring pause is added to the log time. Error log:

Shows the logged error. The last 20 error messages will be stored with date and time. Info:

Tag

: ... Device type

: Control Unit Supplier

: BMA Manufacturer : BMA Device no. Production no. : ...-... Software ver. : V... SW release date: ...

: ... Print Setup:

Printout of the start-up protocol via RS 232 and RS 485. Format, content and example see chapter 9.5 Start- up protocol printout. DynFAS MW 15 Chapter 2 Software Functions 2.2.3 Setup 1 | - | Setup | 07.05 13:25 Configuration Calibration Input / Output Service Product Change password Configuration:

Setup of General data Measurement-specific data Plausibility data Microwave data Marker Units Calibration:

System adjut Concentration calibration Advanced setup Input / Output:

Current outputs Current inputs Pt 100 Digital outputs Digital inputs Service:

In the Profi mode the SERVICE menu is displayed and can be edited. The following settings are possible:

Factory settings General reset Memory Tool (operation of Memory Tool, optional ac-

Data printout (via RS 232 and RS 485, data contents cessory) can be selected) Product:

Product selection (1 4); if you select another product, the product-specific data will be loaded: outputs, inputs and calibration. When you call the products 2 to 4 for the first time, all settings and contents (e.g. system calibration, sampling table, datalog and calibration) of the current product will be copied to the new product. Change password:

The password for the access levels Basic / Profi can be changed here. See for more information also chapter 5 Password. 16 DynFAS MW Chapter 2 Software Functions 2.2.4 Access Level 1 | - | Access Level | 07.05 13:25 Select Level Read only Basic Profi Service ESC ? .... 2.2.5 Language 1 | - | Control Unit | 07.05 13:25 LANGUAGE English German French ESC .. Read only:

word. Basic:

Profi:

This mode can be selected on all levels without pass-

No password required on higher levels. Password has to be entered for Read only. Password can be changed. At the basic level some menu items are disabled, re-

spectively masked, e.g. manual calibration. As described above. Should be used only if you are suf-

ficiently familiar with the measuring system. Changing between basic and profi is possible without using a password. Service:

This level is reserved to the service personnel. Language:

Select the dialog language DynFAS MW 17 Chapter 2 Software Functions 2.2.6 Configuration 1 | - | Configuration | 07.05 13:25 General Data Measurement Plausibility Microwave Marker Units General Data:

Enter date, time and tag Measurement:

Measurement mode (batch/continuous) Start mode (keyboard/external) Averaging (number of measured values used for aver-

Reset average value (yes/no) aging) Plausibility:

The process limits define the valid range, the current concentration has to be within this range. The phase measurement is subject to a plausibility analysis, which can be set here. Enable and define the pause detection. For more information please see chapter 2.2.9 Plausibility Microwave:

Cable (enter the reference and signal cable length). E.g. for 2 meters of HF-cable quad, 4 meters for both length has to be entered. Marker:

You can enter a name (max. 5 characters) and values for a marker. The graphic occurs in the live display and re-

lates to the bar diagram. In order to deactivate the marker, choose a marker value outside of the bar diagram limits or the current output limits. Units:

According the configuration, for the concentration, current input and temperature there are different dimensions se-

lectable. Selectable for concentration are: none, specific, %, %DS, Bx, g/L and g/cm3 18 DynFAS MW Chapter 2 Software Functions 2.2.7 General Data 1 | - | General Datal | 07.05 13:25 Date Time Tag Date:

Enter the current date Time:

Enter the current time Tag:

Enter the tag name. The tag (max. 8 characters) is dis-

played in the header on the display. 2.2.8 Measurement 1 | - | Measurement | 07.05 13:25 Meas. Mode Start Mode Averaging Reset averaging Meas. Mode:

Selection continuous or batch. In batch-mode a mean value is generated from start to stop. In continuous mode a moving average is generated, respective to the mean-

rate preset. Start Mode:

The measurement device can be started or stopped via external terminals (digital input) or via keyboard. Averaging:

Enter the number of single measurement values over which a moving average is to be calculated. Typical: 20 sweeps. Relates only to the measuring mode continuous. Reset Averaging:

Reset averaging (yes/no). Relates to batch or continuous. DynFAS MW 19 Chapter 2 Software Functions 2.2.9 Plausibility Process limits Phase measure Pause detection 1 | - | Plausibility | 07.05 13:25 Process Limits:

A minimum and maximum concentration has to be set. Only concentrations within the range are permitted. If the concentration exceeds the range, the concentration aver-

age is put on hold and an error message is displayed. Phase Measure:

The phase is subject to a plausibility analysis. For more in-

formation please see chapter 2.2.10 Phase Measurement. Pause Detection:

Can be enabled or disabled. Switching variable is the at-

tenuation, if the entered min. attenuation is not reached, the evaluation unit switches to the pause mode:

Current output drops to the lower current output limit

(0/4 mA) Message on display RUN LED is flashing Details regarding pause function see chapter 2.2.11 Pause Detection. 20 DynFAS MW Chapter 2 Software Functions 2.2.10 Phase Measurement Sigma max. Phi/att ratio Auto set 1 | - | Phase measure | 07.05 13:25 Sigma max. Here you set the maximum sigma of the regression Phase vs. Frequency. During normal measurement operation, sigma lies be-

tween 0 and 100. Phi/att ratio The correlation between Phase and Attenuation is another plausibility criterion. It has to be measured when taking the instrument into operation. The automatic ratio meas-

urement is quite helpful (see Auto set). Auto set The automatic ratio measurement Phi/att can be turned on and off. Turn it on during start-up. During measurement, please keep in mind:

Cover the entire concentration range, if possible Do not stop the measurement Do not change the concentration erratically (max. 1 %). Stopping the recording:

The measurement can be stopped by switching off record. The recording is frozen and only restarts when the system switched on again. Start new recording:

Condition: Recording is switched off. Stop and start the measurement before you start a new recording. The re-

sults of old recordings are deleted by doing so. IMPORTANT After the measurement, the automatic measurement has to be disabled again! The ratio value is automatically stored and enabled on the PHI/ATT RATIO menu. DynFAS MW 21 Chapter 2 Software Functions 2.2.11 Pause Detection Enabled Attenuation min 1 | - | Pause detection | 07.05 13:25 no

-15 dB Enabled Here the pause function is activated and deactivated. Con-

sider the measuring conditions for using the pause detec-

tion; see below. Attenuation min Input of the minimum attenuation, when falling below that value measurement goes into pause mode. Conditions and discription:

The pause detection function is a software feature for pause detection between two sequential discontinuous crystallization processes. This is interesting because dur-

ing the cleaning phase, the sensor indicates the lower cur-

rent output value (0/4 mA). Only after restart of a crystal-

lization process, does the sensor show the current dry substance content (Brix content) after product entry. Condition: pure phase calibration first order. This corre-

sponds to the default adjustment of the automatical cali-

bration. For example, a typical signal response from two crystalli-

sation processes. Current output [mA]

Current output [mA]

Pause Pause 0/4 0/4 20 20 t t Necessary Software Installations Enter under menu SETUP | CONFIGURATION | PLAUSIBIL-

ITY | the following values:

Under PROCESS LIMITS:

Min. Conc. and Max. Conc. Entry of process limits: 5 %DS to the real process limits. Example: real process limits 70 to 90 %DS, therefore 65 to 95 %DS is entered. Under PAUSE DETECTION:

The pause detection can be activated here. Switching variable is the attenuation; if the entered minimum attenuation is fallen short of, then the evaluation unit pauses.

22 DynFAS MW Chapter 2 Software Functions Adjust these settings if applicable according to the condi-

tions of Quitting the pause mode (see below). Determination of the min. attenuation as a switching variable:

0 0 D1 D1 D2 D2 For this, the attenuation process must be observed up to the end of a crystalliza-tion process including cleaning phase. In addition, you can take the data log (see chapter 2.2.2 diagnosis) for assistance. For example, a typical attenuation process:

Attenuation [dB]

Attenuation [dB]

D1 = smallest attenuation value in the product D2 = Attenuation value for an empty vessel D (min) = Switching variable = average attenuation be-

tween D1 and D2 Typical values (Sugar beet):

D1: -15 to -10 dB D2: -25 to -20 dB D (min): -20 to -15 dB Pause Pause t t Quitting the pause mode (change to measuring mode):

Two conditions have to be met before changing the mode:

The attenuation has to be higher than the attenua-

1. tion threshold. The recent concentration (Conc act.) has to be in the following range:

Conc act.> min. process limit Conc act.< min. process limit A1Faktor146 2. A1:

Factor:

Process limit:

Calibration coefficient of the phase From tuning (Default =1; see chapter 2.2.13 Calibr. Concentration). See menu PLAUSIBILITY DynFAS MW 23 Chapter 2 Software Functions 2.2.12 Calibration 1 | - | Calibration | 07.05 13:25 System Adjust Calibrate Conc Calibrate Conc2 Advanced System Adjust:

The system calibration is started on this page. Calibrate Conc:

Opens the calibration menu of concentration 1 Calibrate Conc2:

Opens the calibration menu of concentration 2 Advanced:

Here you set the Tara values, number of sweeps at sam-

pling, process type and split value. Details see chapter 2.2.17 Advanced. 2.2.13 System Adjust 1 | - |System Adjust | 07.05 13:25 Adjust Num. Sweeps Reference values Chart Phi Chart Attnuation Adjust:

System calibration is started. Num. Sweeps:

Here you define the number of sweeps for the system ca-

libration (arithmetic mean value). Ref. values:

Upon completion of the reference measurement, the ref-

erence values for phase, attenuation, slope and sigma can be output. Chart Phi:

Shows the characteristic curve of Phase versus Frequency based on the regression. Chart Attenuation:

Shows the characteristic curve of Attenuation versus Fre-

quency based on the regression. By means of a system calibration, the data log is not deleted

(see chapter 2.2.2 Diagnosis). 24 DynFAS MW Chapter 2 Software Functions 2.2.14 Calibrate Concentration 1 | - |Calibrate Conc| 07.05 13:25 Sampling Calibr. autom. Calibr. manual Tuning View Sampling:

Shows all measured samples. Calibr. autom.:

Calibration can be started after measurement of two sam-

ples and input of the respective laboratory values. More-

over, compensation can be enabled if the following pre-

requisites have been fulfilled:

1. The respective analog input has been enabled (Pt100 or current input 1 / 2). 2. Sampling has been carried out using the previously set up compensation input. 3. The reference value has been entered on the menu COMPENSATION. The reference value is either the current product temperature at system adjustment or the average product temperature. There are at least three samples needed for temperature compensation, otherwise the calibration error Keeping old coefficients appears at the evaluation unit. Basis of automatic calibration (fixed setting):

Linear phase calibration Compensation: additive and linear Calibr. manual:

Here you can choose the calibration order [lin-

ear/quadratic], the basis [phase/attenuation or both] and compensation temperature. Tuning:

Subsequent correction of the reading is possible by enter-

ing a factor and an offset. Calculation is carried out according to the following for-

mula:

Corrected display

display factor

offset View:

Presentation of calibration curve, display of correlation and coefficients. DynFAS MW 25 Chapter 2 Software Functions 2.2.15 Sample No. 1 | 1/1 | Sample # 1 | 07.05 13:25 DEL .... Next sample Active Measured value Lab value Advanced Yes 65.50 %

0.00 %

The header includes the following information (starting from the left):

Product-No. Current table position / Total number of entries Sample no. of current table position Date and time of sampling Up to 20 sample entries are possible. The sample can be as-

signed to the lab value either via the sample no. or via date/time. The sample no. is assigned on a continuous basis. If a sample is deleted, the sample no. will not be assigned a second time. Up to 999 sample numbers are available. Only if all numbers have been assigned, you may assign a number for the second time; you will be alerted accordingly on the display. Next sample:

Continues with the next sample. Active:

Here you can choose if this sample should be taken into account for calibration. Measured value:

Display of the measured values, calculated with the ac-

tual coefficient. Lab value:

Entry position for the laboratory value. Advanced:

Switches to the next data page. DEL:

The displayed sample value can be deleted by pushing briefly the corresponding soft key. Pushing longer, all sample values are deleted at once. DynFAS MW 26 Chapter 2 Software Functions 2.2.16 Sample Data (expanded) 1 | 1/1 | Sample # 1 | 07.05 13:25 DEL .... Current In 1 Current In 2 PT100 PHI (m) Attenuation Current In 1:

Editable display of the first compensation input. Current In 2:

Editable display of the second compensation input. Pt 100:

Editable display of the Pt 100 input. PHI (m):

Not editable display of the measured phase. Attenuation:

Not editable display of the measured attenuation. 2.2.17 Advanced Settings 1 | - | Advanced | 07.05 13:25 Tara values Num. Cal. Sweeps Process type Split Value Tara Values:

Input option of Tara values for phase and attenuation. The Tara values are attributed to the phase or the attenuation before calibration. The calculation is the following:

Phase = Phasemeas - Phase Tara Attenuation = Attunationmeas - AttenuationTara This function is not needed for the determination of dry substance, brix or density in sugar solution. Number of Calibration Sweeps:

Freely adjustable number of sweeps over which a calibra-

tion point (in the course of automatic sample measure-

ment) will be averaged. Process Type:

Select the operation mode:

one concentration [1 measuring range]

two concentrations [2 measuring ranges]

split concentration [1 measuring range with switching point (split value) for coefficient switchover]. Split Value:

Setting of the switching point on a value basis. DynFAS MW 27 Chapter 2 Software Functions 2.2.18 Calibr. manual 1 | - | Calibr. manual | 07.05 13:25 Cal. Order Cal. Base Coefficients Compensation Start Calibr. Cal. Order:

Here you define the calibration order [linear / quadratic]

Cal. Base:

The following parameters can be set:

Phase Attenuation Phase and attenuation Coefficients:

Here you can edit all coefficients for phase and attenua-

tion. Compensation:

If at least one analog input is active, you may assign the compensation and set the compensation parameters. Start Calibr.:

Starts the calibration using the parameters you have set earlier. 2.2.19 Input / Output 1 | - | Inputs/Outputs | 07.05 13:25 Current Output Current Input PT100 Digital Output Digital Input Current Output:

Both outputs can be adjusted, assigned and set up on the selected level. Current Input:

Activation level of current input, calibration and display of the live current signal. Pt 100:

Here you can enable and adjust a connected Pt 100. Dis-

play of the actual temperature signal. Digital Output:

Allocation of relays 1 and 2 and test function. Digital Input:

Status control and assignment of the digital inputs. 28 DynFAS MW Chapter 2 Software Functions Current Out 1:

Selection of input dialogue for output 1. Current Out 2:

Selection of input dialogue for output 2. 2.2.20 Current output 1 | - | Current Output | 07.05 13:25 Current Out 1 Current Out 2 2.2.21 Current Output 1 1 | - | Current Out 1 | 07.05 13:25 Assignment Upper value Lower value Test / Adjust Error current Assignment:

The current output can be assigned to a concentration or one of the activated inputs. Upper value:

Display value assigned to the 20mA value. Lower value:

Display value assigned to the 4mA value. Tip Current output 1 only 4 20mA possible Test/Adjust:

Current test, calibration and display of live current. IMPORTANT In case of test function, the measurement should be stopped. Error current:

Status of current output in case of error 22 mA 3.5 mA Hold Value DynFAS MW 29 Chapter 2 Software Functions 2.2.22 Current Output 2 1 | - | Current Out 2 | 07.05 13:25 Assignment Upper value Lower value Range Test / Adjust Error current 2.2.23 Current input 1 | - | Current Input | 07.05 13:25 Current In 1 Current In 2 2.2.24 Current In 1 1 | - | Current In 1 | 07.05 13:25 Enabled Adjust Live current All functions same as current output 1 Tip Current output 2 can be set from 0 20mA to 4 20mA. Range:

Change of the current output 0 20mA 4 20 mA Current Input 1:

When selected, change to activation and calibration menu. Current In 2:

As described above. Enabled:

If you select yes/no, the current input is enabled or dis-

abled. Adjust:

Follow the instructions on the display. Live current:

Display of the live current signal. 2.2.25 Current In 2 Set and enabled same as input 1. 30 DynFAS MW Chapter 2 Software Functions 2.2.26 Pt 100 1 | - | Pt 100 | 07.05 13:25 Enabled Trim Pt 100 Pt 100 live 2.2.27 Digital Output 1 | - | Digital Output | 07.05 13:25 Relay 1 Relay 2 Test 2.2.28 Digital Input 1 | - | Digital Input | 07.05 13:25 Status DI 1 function DI 2 function DI 3 function Enabled:

If a Pt 100 is connected, the input has to be enabled first. Trim Pt 100:

You need a 100 Ohm and a 138.5 Ohm resistance. Follow the instructions on the display. Pt 100 live:

Display of the live temperature. Relay 1:

Relay 1 can be assigned to different functions:

None Error Halt No product Alarm min. Alarm max. Relay 2:

Same assignments possible as above. Test:

The switching status of the relays can be set here and checked at the respective terminals. Status:

Shows the status of the input circuit open/closed DI 1 Function:

The following functions can be assigned to DI 1:

None Start (external start) DI 2 Function:

The following functions can be assigned to DI 2:

None Hold (averaging is stopped) Product (external product selection) DynFAS MW 31 Chapter 2 Software Functions 2.2.29 Service 1 | - | Service | 07.05 13:25 Factory setting General reset Memory Tool Data printout DI 3 Function:

Assignments for DI 3 None Sample (external control of sampling) Product (external product selection) Factory Settings and general reset:

See table on next page. Memory Tool:

Communication with the external memory unit (Memory Tool, optional accessory). Data transfer takes place via the 9-pole SubD-connector on the bottom of the instrument. Backup settings: all operation parameters for all prod-

ucts are stored in the Memory Tool. Upload settings: all operation parameters are loaded into the evaluation unit by the Memory Tool. With that, all parameters are deleted from the evaluation unit. Backup data log: the data log is stored on the Memory Backup setup: the start-up protocol is stored on the Tool. Memory Tool. 32 The concentration average value is put on hold during communica-

tion with the Memory Tool. With this, the measured value from the current output is also frozen!

Data Printout:

All measurement values for every single measurement

(sweep) are sent by the serial interfaces RS 232 and RS 485 (also referred to as raw data). The output can be adjusted as follows:

None (disabled) Row (data transfer, see Hardware Manual chapter 6.4) Table (microwave data for each frequency point) Row and table (one data row and one table are output for each sweep) Default represents Line. DynFAS MW Chapter 2 Software Functions Language selection Access level Measurement Password Product selection Error log Data log Factory settings Unchanged Unchanged Has been stopped Unchanged Unchanged Not deleted Not deleted, Setting default Not deleted Unchanged Not deleted System calibration Cable length Sample table Measuring table description Default All parameter under menu:

Default Measurement Plausibility Marker Unit Calibration coefficients All calibration under the analog and digital in and outputs. Adjustment of analog in and outputs Remark:

Default Default

Unchanged Only is effective on current product General Reset Unchanged Default: Basis Has been stopped Default: PASS1 All products deleted Deleted Deleted, setting de-

fault Deleted Default Deleted Default Default Default Default Deleted Is effective for all products (P1 to P4)

*Default: default values, see chapter 9. under Factory settings DynFAS MW 33 Chapter 2 Software Functions 2.3 Trend Display 1 | - | Live Display | 07.05 13:25 Concentration av. 43.20 %

Conc av. Act. 45 %

ESC SAMPLE ZOOM

| | Concentration av. |

MIN Push the ZOOM button to enlarge the measurement value which is surrounded by a frame. By pushing the ZOOM button for a longer time, the enlarged measurement value will be displayed as trend over the entire display. The trend display corresponds to the contents of the datalog. Datalog has to be enabled for the trend display. During the trend set up (few seconds), the measuring value or the power output is frozen. 34 DynFAS MW Chapter 3 Configuration Chapter 3. Configuration Before carrying out any calibration work, you should check the configuration setup of the measuring system and change it, if necessary. 3.1 Configuration Setup 1 | - | Setup | 07.05 13:25 Configuration Calibration Input / Output Service Product Change password 3.1.1 General Data 1 | - | Configuration l | 07.05 13:25 General Data Measurement Plausibility Microwave Marker Units 1 | - | General Datal | 07.05 13:25 07.05.2004 13:25 App.1 Date Time Tag 1 | - | General Data | 07.05 13:25 Date 07.05.2004 |

ESC ..?.. DEL ....

CONFIGURATION

GENERAL DATA Example:

Select the respective entry, edit and store it.

DATE Push DEL to delete the entry and then enter the new date. Push.... to confirm and store the changed date. Tip The colon for the time input (e.g. 13:25) is invoked by pushing the button [ . ]. DynFAS MW 35 Chapter 3 Configuration 3.1.2 Measurement 1 | - | Measurement | 07.05 13:25 Meas. Mode Start Mode Averaging Reset Averaging Continuous Keypad 20 no 3.1.3 Plausibility Process Limits Phase Measure Pause Detection 1 | - | Plausibility | 07.05 13:25 3.1.4 Microwave 1 | - | Microwave | 07.05 13:25 Cables Ref. cable length Signal cable length 1 | - | Cables | 07.05 13:25 4 m 4 m You have to check the settings on this display and adapt them to the measurement conditions. For example, you have to adapt the measurement mode, the start mode and the averaging to the actual operating condi-

tions. To rule out any unnecessary disturbances during calibration, the process limits should be set, as far as possible, below or above the measuring range. You should keep the factory-set default values for the phase measurement and disable Pause detection. If a default value has to be changed, you have to check all entries that are relevant for calibration and, if necessary, renew them. Upon completion of the calibration work, you can enable Pause detection again.

CABLES If the factory-set cable lengths do not match the actual geome-

try conditions, you have to correct the values. Example: For a 2 m long HF quad cable, enter 4 m for the reference and signal cable length. The input value corre-

sponds to twice the quad cable length. 36 DynFAS MW 3.1.5 Marker 1 | - | Configuration | 07.05 13:25 General Data Measurement Plausibility Microwave Marker Units 3.1.6 Units 1 | - | Configuration | 07.05 13:25 General Data Measurement Plausibility Microwave Markers Units 1 | - | Units | 07.05 13:25 Conc Conc 2 Current in 1

% TS

C Chapter 3 Configuration You can set a marker comprising max. 5 characters which identify the value set on in the live display.

MARKER Set the units as desired.

UNITS

CONC The units of the concentrations (conc 1 and 2) and those of the enabled analog inputs can be selected. 1 | - | Units | 07.05 13:25 Conc. None Specific

% DS Bx

ESC ..?.. .... Different units can be set for both concentrations. DynFAS MW 37 Chapter 3 Configuration 1 | - | Units | 07.05 13:25 Conc Conc 2 Current in 1

% TS

C 1 | - | Units | 07.05 13:25 Current in 1 None Specific C F ESC ..?.. ....

CURRENT INPUT 1

C The temperature input can be set to C, F, specific or none. 38 DynFAS MW Chapter 3 Configuration 3.2 Start Calibration Coefficients 1 | - |Calibrate Conc| 07.05 13:25 Sampling Calibr. autom. Calibr. manual Tuning View 1 | - | Calibr. manual | 07.05 13:25 Cal. Order Cal. Basis Linear PHI Coefficients Compensation Start Calibration 1 | - | Coefficients | 07.05 13:25 0 50 A1 C Prerequisite: You are in the Profi mode If the display depicted to the left is not visible, do the follow-

ing on the live display:

ESC | SETUP | CALIBRATION | CALIBRATE CONC |

CALIBR. MANUAL

COEFFICIENTS The concentration is calculated as follows:

Con = A1 + C with = Phase Check the coefficients A1 and C and correct them, if neces-

sary, as follows:

C = average measuring range value (concentration value) A1 = 0 Note: With these calibration coefficients the concentration aver-

age value and thus the current output is put on hold during start-up. DynFAS MW 39 Chapter 4 Calibration Chapter 4. Calibration Note: The measuring system has been connected properly and the normal operating temperature has been reached (approx. 30 to 45 min. acclimatization). It has to be ensured that the flow cell is completely filled with product or the container probe is completely surrounded by pro-

duct. Prerequisite: Chapter 3.1 Configuration Setup has been completed. 4.1 System Calibration 1 | - | Control Unit | 07.05 13:25 Live Display Diagnostic Setup Access Level Language Basic English If you turn on the measuring system, the following display appears:

SETUP RUN 1 | - | Setup | 07.05 13:25 Configuration Calibration Input / Output Product Change password 1 | - | Calibration | 07.05 13:25 System Adjust Calibrate Conc

CALIBRATION

SYSTEM ADJUST DynFAS MW 41 Chapter 4 Calibration 1 | - | System Adjust | 07.05 13:25 Adjust Num. Sweeps 10 1 | - | System Adjust | 07.05 13:25 System adjustment now?

..X.. .... 1 | - | System Adjust | 07.05 13:25 Adjustment in process ... . .......................................... 1 | - | System Adjust | 07.05 13:25 Adjusted!

..OK.. The manufacturer has set the number of measurement cycles

(sweeps) to 10.

ADJUST Confirm System adjustment is in process. Push ..OK.. to confirm and push three times to return to the main menu. 42 DynFAS MW Chapter 4 Calibration 4.2 Start-up of CH-200 total attenuation attenuation while system adjustment actual attenuation while measuring The system adjustment and the calibration shall be carried out for the high dynamic version of CH-200 as well as for the Standard Model CS-100. However, it is important to note that the CH-200 requires a minimum attenuation of 40 dB over the entire concentration range and for system adjust-

ment. When falling below, the measurement is not precise anymore and error prompts may occur. The complete attenuation is generated the following way:

dB total = dB adjust + dB live + 0.4 x measuring cable length This applies for:

dBtotal :

dBadjust:

dBlive:

measuring cable length: e.g. 4 meters of HF-cable quad re-

sults into 8 meters measuring cable length (counting both ways, forward and backwards). The software sends an error message if there is a shortfall in attenuation and the Control Unit enters error state (error No. 55). Remedy when falling below minimum attenuation:

If the necessary attenuation is not reached, it is possible to install a 10 dB attenuator in the transmitter branch (see Fig-

ure 4-1). However when falling below significantly, the stan-

dard system CS-100 should be used instead. N-attenuator 10dB CA-100 M-Rx M-Tx R-Rx R-Tx Figure. 4-1:

Installation the 10 dB attenuator HF-cable quad x R M

x T

M x T

R x R

R DynFAS MW 43 Chapter 4 Calibration 4.3 Start Calibration 1 | - | Control Unit | 07.05 13:25 Live Display Diagnostic Setup Access Level Language Basic English RUN 1 | - | Run / Stop | 07.05 13:25 Switch operating mode?

..X.. .... Push RUN to start the measuring system. Push .... to confirm this prompt and the instrument switches to the run mode. 4.3.1 First Process Run Prerequisite: You are in the Profi mode Chapters have been completed. 3.1 Configuration Setup 3.2 Start Calibration Coefficients 4.1 System Calibration The first process run is used to determine the ratio of Phase and Attenuation (Phi/att), a parameter from the plausibility analysis for correct determination of the phase. If you know the ratio already from other measurements, you may enter it directly on the PLAUSIBILITY menu (see chapter 2.2.10 Phase Measurement); in this case, process recording is not necessary. IMPORTANT The measurement takes place automatically; you only have to start and stop it again. During measurement, please keep in mind:

- Do not stop the measurement

- Do not change the concentration erratically (max. 1%).

- Cover the entire measuring range, if possible DynFAS MW 44 Chapter 4 Calibration Process Limits Phase Measure Pause Detection 1 | - | Plausibility | 07.05 13:25 1 | - |Phase Measure | 07.05 13:25 Sigma max. Phi/att ratio 100.00 6.00 OFF Auto set 1 | - |Phase Measure | 07.05 13:25 Auto set Off On ESC ..?.. .... 1 | - |Phase Measure | 07.05 13:25 Sigma max. Phi/att ratio 100.00 5.32 ON Auto set From the main menu, you get in the Advanced mode to the display to the left by selecting | SETUP | CALIBRATION |

CALIBRATE CONC.

PHASE MEASURE

AUTO SET

ON While the process recording is running, carry out sampling (see the following chapter). Do not forget to enable the process recording again as described above!

DynFAS MW 45 Chapter 4 Calibration 4.3.2 Sampling Average concentr. 1 | - | Live Display | 07.05 13:25 Conc av. Conc. act. 64.35%

ESC SAMPLE .... ZOOM 65.50 %

1 | - | Live Display | 07.05 13:25 Taking Sample #1 Conc av. Conc act 64.35%

..X.. .... Save sample no. 1?

1 | - | Live Display | 07.05 13:25 Conc av. Conc act 64.35%

. .X.. .... .... Push RUN and the display to the left will appear. Note: Push the SAMPLE button to start measurement of the raw data. At the same time, the laboratory sample has to be taken and marked. The analysis may be performed later, provided the product is not changed by this. Sampling is in process...... Push the ..X.. button to stop the sampling process any time. If the sampling process has been completed without any problem, push the .... button to save the sample in the ta-

ble and the measurement continues. You have to repeat the process described above for each further sample. The second sample taking should be started only when the dis-

play shows a significant difference to the first sample taking. The assumed concentration of the samples should be distributed within the complete measuring range. If there is an additional temperature compensation, the temperature of the samples should be also distributed within the complete temperature range. The minimum number of required samples is derived according to the preset calibration. In case there is not a sufficient number of samples, an error message will appear after attempted cali-

bration. 46 DynFAS MW Chapter 4 Calibration 4.3.3 Entering the Lab Values Average concentr. 65.50 %

1 | - | Live Display | 07.05 13:25 Conc av. Act. Conc. 64.35%

ESC SAMPLE .... ZOOM Push the ESC button to go to the main menu. A measure-

ment can be stopped only on the main menu. Push STOP to stop the measuring system. Push .... to confirm the prompt and the measurement swit-

ches to the STOP mode.

SETUP

CALIBRATION 1 | - | Control Unit | 07.05 13:25 Live Display Diagnostic Setup Access Level Language Basic English STOP 1 | - | Start / Stop | 07.05 13:25 Switch operating mode?

..X.. .... 1 | - | Control Unit | 07.05 13:25 Live Display Diagnostic Setup Access level Language Basic English RUN 1 | - | Setup | 07.05 13:25 Configuration Calibration Input / Output Service Product Change password DynFAS MW 47 Chapter 4 Calibration 1 | - | Calibration | 07.05 13:25 System Adjust Calibrate Conc Advanced 1 | - | Calibrate Conc| 07.05 13:25 Sampling Calibr. autom. Calibr. manual Tuning View 1 | 1/1 | Sample # 1 | 07.05 13:25 Next sample ActiveYes Measured value Lab value Advanced

.. . DEL .... 65.50 %

0.00 %

1 | 1/1 | Sample # 1 | 07.05 13:25 Lab value 0.00| %

ESC ..?.. DEL .... 1 | 1/1 | Sample # 1 | 07.05 13:25 Next sample ActiveYes Measured value Lab value Advanced

.. . DEL .... 65.50 %

72.40 %

CALIBRATE CONC

SAMPLING

LAB VALUE Delete default value with DEL, enter new value and confirm with .....

NEXT SAMPLE and repeat the step described above with the next sample. After you have entered the last sample by pushing the but-

ton you get back to the Calibration menu. (Short push one page, longer push of the button you get back to the Calibra-

tion menu immediately.) 48 DynFAS MW Chapter 4 Calibration 4.3.4 Automatic Calibration 1 | - |Calibrate Conc | 07.05 13:25 Sampling Calibr. autom. Tuning View 1 | - |Calibrate Conc | 07.05 13:25 Start Calibr. 1 | - |Calibrate Conc | 07.05 13:25 Calibrate now?

..X.. .... 1 | - |Calibrate Conc | 07.05 13:25 Calibrated!

..OK.. 1 | - |Calibrate Conc | 07.05 13:25 Sampling Calibr. autom. Tuning View Phase calibration including the enabled compensation is carried out during automatic calibration.

CALIBR. AUTOM.

START CALIBR. Push the .... button to start the calibration. Push the ..OK.. button to confirm calibration. When calculating the new coefficient set, factor and offset will be reset (factor 1.00000 and offset 0.000). Push the button four times to return to the main menu. DynFAS MW 49 Chapter 4 Calibration 4.3.5 Automatic Calibration with Temperature Compensation Before running a sample measurement you have to enable the desired compensation input and check the calibration. If all in-

puts are enabled, the measured values of all inputs will be sto-

red automatically in the sample table. Usually, automatic calibration is sufficient and can be per-

formed in the Basic mode. The chapters 4.1 System Calibration 4.2.2 Sampling and 4.2.3 Entering of Lab Values are prerequisites for automatic calibration. Starting from the main display, you get to the display de-

picted to the left by selecting | SETUP | CALIBRATION |

CALIBRATE CONC. |

CALIBR. AUTOMATIC

COMPENSATION All active inputs are displayed here for compensation selec-

tion.

CURRENT IN 1 1 | - |Calibrate Conc | 07.05 13:25 Sampling Calibr. autom. Tuning View 1 | - | Calibr. autom. |07.05 13:25 Start Calibr. Compensation None 1 | - | Calibr. autom. | 07.05 13:25 Compensation None Current In 1 PT100 ESC ..?.. .... 50 DynFAS MW Chapter 4 Calibration 1 | - |Calibr. autom. |07.05 13:25 Start Calibr. Compensation Current In 1 Ref. value 1 | - | Compensation | 07.05 13:25 Ref. value 80.00 |

C ESC ..?.. DEL .... 1 | - | Calibr. autom. |07.05 13:25 Start Calibr. Compensation Current In 1 Ref. value 80 C 1 | - | Calibr. autom. | 07.05 13:25 Calibrate Now?

..X.. .... 1 | - | Calibr. autom. | 07.05 13:25 Calibration in process.. .OK.. 1 | - | Calibr. autom. | 07.05 13:25 Calibrated!

..OK..

REFERENCE VALUE After selection of the compensation input, REFERENCE VALUE is displayed on the menu. The input of a reference value

(e.g. the reference temperature) is required. As reference value either the temperature of the product dur-

ing calibration or the averaged operating temperature en-

tered and confirmed.

START CALIBRATION Start calibration. Push ..OK.. to confirm the Calibration. The calibration is fin-

ished. Push the Home button four times to return to the main menu and to start a measurement. DynFAS MW 51 Chapter 4 Calibration 4.4 Manual Calibration Manual calibration is possible only on the Profi level. Prerequisite a for manual calibration are the chapters 4.1 System Calibration 4.2 Start Calibration 4.2.2 Sampling and 4.2.3 Entering the Lab Values 4.4.1 Manual Calibration with one Concentration 1 | - | Calibrate Conc| 07.05 13:25 Sampling Calibr. autom. Calibr. manual Tuning View 1 | - | Calibr. manual | 07.05 13:25 Linear PHI Cal. Order Cal. Base Coefficients Start Calibr. 1 | - | Calibr. manual | 07.05 13:25 Cal. Order Linear Quadratic If the display depicted to the left is not visible, do the follow-

ing on the live display:

ESC | SETUP | CALIBRATION | CALIBRATE CONC |

CALIBR. MANUAL

CAL ORDER

LINEAR Quadratic calibration is possible only for a calibration with three and more samples. DynFAS MW 52 Chapter 4 Calibration 1 | - | Calibr. manual | 07.05 13:25 Cal. Order Cal. Base Linear PHI Coefficients Start Calibr. 1 | - | Calibr. manual | 07.05 13:25 Cal. Base Phase Attenuation Both

CAL. BASE

PHASE (Phase measurement) ESC ..?.. .... The calibration base is selected depending on the number of samples and their raw data. Initial calibration should be as sim-

ple as possible, since calibration can be optimized any time. 1 | - | Calibr. manual | 07.05 13:25 Cal. Order Cal. Base Coefficients Start Calibr. Linear PHI 1 | - | Calibration | 07.05 13:25 Calibrate Now?

..X.. .... 1 | - | Calibration | 07.05 13:25 Calibrated!

..OK..

START CALIBRATION Push .... to start the calibration, push ..X.. to go back one page without calibration. .OK.. takes over the calibration and changes to the next dis-

play. DynFAS MW 53 Chapter 4 Calibration 1 | - | Calibration | 07.05 13:25 Lab 1 | - | Calibration | 07.05 13:25 Correlation Lab/Meas value 0.998726

..OK.. 1 | - | Calibration | 07.05 13:25 Calibration OK?

..X.. .... The curve to the left shows the characteristic curve lab vs. measured value.

.... The correlation shows the average deviation of the character-

istic curve from the sample series.

..OK.. As soon as you confirm this prompt, the calibration display appears again; from there you get back to the main menu by pushing four times and you can start the measurement again. 54 DynFAS MW Chapter 4 Calibration 4.4.2 Calibration with Two Concentrations Calibration for two concentrations starts by changing the proc-

ess type as described below. Prerequisite for calibration are the chapters 4.1 System Calibration and 4.2.2 Sampling 1 | - | Calibration | 07.05 13:25 System Adjust Calibrate Conc Advanced 1 | - | Advanced | 07.05 13:25 Tara values Num. Cal. Sweeps 10 Process Type 1| - | Advanced | 07.05 13:25 Process Type 1 Conc 2 Conc Split Conc. ESC ..?.. .... 1 | - | Calibration | 07.05 13:25 System Adjust Calibrate Conc Calibrate Conc 2 Advanced

ADVANCED

PROCESS TYPE

2 CONC Push the .... button to accept the selected process type and push the button once to go to the display depicted below.

CALIBRATE CONC 1 DynFAS MW 55 Chapter 4 Calibration 1 | - | Calibrate Conc1|07.05 13:25 Sampling Calibr. autom. Calibr. manual Tuning View 1 | 1/4 | Sample # 1 | 07.05 13:25 Next sample Active Measured value Lab value Advanced DEL .... Yes 65.50 %

0.00 %

Lab value 1 | 1/4 | Sample # 1 | 07.05 13:25 60.40 |

ESC ..?.. DEL .... 1 |1 /4 | Sample # 1 | 07.05 13:25 Next sample Active Meas. value Lab value Advanced DEL .... Yes 65.50 %

60.40 %

1 |2 /4 | Sample # 2 | 07.05 13:25 Next sample Active Meas. value Lab value Advanced DEL .... Yes 74.35 %

67.80 %

SAMPLING There is only one sample table for both calibrations. The lab values have to be entered for all samples used for cali-

bration of concentration 1. All other samples have to be disabled

(Active.... Yes/No).

LAB VALUE Delete default value with DEL, enter new value and confirm with .....

NEXT SAMPLE Continue with next sample

ACTIVE Disable sample 56 DynFAS MW Chapter 4 Calibration 1 | 2/4 | Sample # 2 | 07.05 13:25 Active No Yes ESC ..?.. DEL .... 1 |2 /4 | Sample # 2 | 07.05 13:25 DEL .... Next sample Active Meas. value Lab value Advanced No 74.35 %

67.80 %

1 | - | Calibrate Conc1|07.05 13:25 Sampling Calibr. autom. Calibr. manual Tuning View 1 | - | Calibr. autom. |07.05 13:25 Start Calibr. 1 | - | Calibr. autom. | 07.05 13:25 Calibrate Now?

..X.. ....

NO Make sure that all samples have been processed and only those samples are active which are relevant for this calibration. Push ESC to get to the Calibration page Automatic as well as manual calibration is possible in this cali-

bration mode. We recommend the automatic mode for begin-

ners.

START CALIBRATION Push .... to start the calibration, push ..X.. to go back one page without calibration. DynFAS MW 57 Chapter 4 Calibration

..OK.. takes over the calibration and changes to the next dis-

play. Push twice to return two pages.

CALIBRATE CONC 2 Repeat the steps as described above for concentration 2; all samples have to be enabled again in the sample table. Now you have to disable all samples which are not used for concentration 2.

SAMPLING 1 | - | Calibr. autom. | 07.05 13:25 Calibrated!

..OK.. 1 | - | Calibr. autom. |07.05 13:25 Start Calibr. 1 | - | Calibration | 07.05 13:25 System Adjust Calibrate Conc Calibrate Conc 2 Advanced 1 | - |Calibrate Conc2 | 07.05 13:25 Sampling Calibr. autom. Calibr. manual Tuning View 58 DynFAS MW Chapter 4 Calibration 4.4.3 Calibration with Split Value With this type of calibration, two characteristic curves (con-

centrations) are combined in one measuring range; their point of intersection defines the split value. Conc 1 for the lower and conc 2 for the upper measuring range can be output only together via current output.

ADVANCED

PROCESS TYPE

SPLIT CONC Push the .... button to accept the selected process type and push the button once to go to the display depicted below. The displayed split value has been set by the manufacturer, but has to be adapted to the respective application. The samples should be chosen that way that the last sample of the lowest concentration is as close as possible to the first sam-

ple of the highest concentration. It is the ideal case, when the last sample of the initial concentra-

tion coincides with the first sample of the final concentration. 1 | - | Calibration | 07.05 13:25 System Adjust Calibrate Conc Advanced 1 | - | Advanced | 07.05 13:25 Tara values Num. Cal. Sweeps 10 Process Type 1 | - | Advanced | 07.05 13:25 Process Type 1 Conc 2 Conc Split Conc ESC ..?.. .... 1 | - | Advanced | 07.05 13:25 Tara values Num. Cal. Sweeps 10 Split Conc 75.00 %

Process Type Split Value DynFAS MW 59 Chapter 4 Calibration Concentration av. 65.50 %

1 | - | Live Display | 07.05 13:25 Conc av. Conc. act. 64.35%

ESC SAMPLE .... ZOOM 1 | - | Advanced | 07.05 13:25 Tara values Num. Cal. Sweeps Process Type 10 Split Conc 75.00 %

Split Value 1| - | Advanced |07.05 13:25 Split Value 75.00 |

ESC ..?.. DEL .... 1 | - | Calibration | 07.05 13:25 System Adjust Calibrate Conc Calibrate Conc 2 Advanced The sample measurement is carried out continuously over the entire measuring range with the display depicted to the left. See chapter 4.2.2 Sampling After completion of sampling, the individual samples will be enabled or disabled during input of the laboratory values, relative to the set split values. All samples smaller or equal to the split value will be assigned to the lower concentration range and all samples above to the upper concentration range. The correlation of the samples is carried out automatically, for instance after setting the splitting value or after entering the laboratory value (e.g. after re-sampling). The correlation complies with both, the splitting value and the laboratory value. IMPORTANT By entering a splitting value, this automatic correlation reac-

tivates samples that had been deactivated before! In such cases the deactivated samples should be deleted or deacti-

vated again after entering the splitting value. The required splitting value has to comply with the intersection of the two calibration characteristic lines. After calibration it is adjusted automatically (only to a certain extend).

SPLIT VALUE Enter the split value and confirm with ..... Push the Home button to return to the calibration page.

CALIBRATE CONC 60 DynFAS MW Chapter 4 Calibration 1 | - |Calibrate Conc2|07.05 13:25 Sampling Calibr. autom. Calibr. manual Tuning View

CALIBR. AUTOM. The lower concentration is now calibrated. Then select CONC 2 and repeat the calibration process. Back to the main menu and start the measurement. 4.4.4 Calibration with Temperature Compensation 1 | - | Calibrate Conc | 07.05 13:25 Sampling Calibr. autom. Calibr. manual Tuning View 1 | - | Calibr. manual | 07.05 13:25 Cal. Order Cal. Base Coefficients Linear Phase Compensation Start Calibr. 1 | - | Compensation | 07.05 13:25 Input Mode Order Ref. value C_Phi 1 C_dB 1 None Additive Linear 0.00 0.00000 0.00000 ESC ..?.. .... 1 | - | Calibrate Conc | 07.05 13:25 Input None Current In 1 Current In 2 PT100 Starting from the main menu, you get to the display to the left by selecting | SETUP | CALIBRATION | CALIBRATE CONC

| in the Profi mode.

CALIBR. MANUAL

COMPENSATION

INPUT If all inputs have been enabled during sample measurement, you have the option to select compensation from the list, since all input values have been stored in the sample table.

Pt 100 DynFAS MW 61 Chapter 4 Calibration You can select additive or multiplicative mode and set the or-

der to linear or quadratic. If you select automatic calibration mode, the above modes will be calculated automatically. This is recommended for non-professional users.

REF VALUE As reference value either the temperature of the product dur-

ing calibration or the averaged operating temperature en-

tered and confirmed. The coefficients C_Phi 1 and C_dB 1 are automatically calcu-

lated during calibration.

ESC If you have completed the entries described above and have carried out the steps described in chapters 4.1 System Calibration 4.2.2 Sampling and 4.2.3 Entering the Lab Values you may proceed with the calibration as described below.

START CALIBR. DynFAS MW 1 | - | Compensation | 07.05 13:25 Input Pt 100 Mode Order Ref. value C_Phi 1 C_dB 1 Additive Linear 0.00C 0.00000 0.00000 ESC ..?.. .... 1 | - | Compensation | 07.05 13:25 Ref. value 80.00 |

C ESC ..?.. DEL .... 1 | - | Compensation | 07.05 13:25 Additive Linear 80.00C 0.00000 0.00000 ESC ..?.. .... Input Pt 100 Mode Order Ref. value C_Phi 1 C_dB 1 1 | - | Calibr. manual | 07.05 13:25 Cal. Order Cal. Base Coefficients Compensation Linear Phase Start Calibr. 62 Chapter 4 Calibration 1 | - | Calibration | 07.05 13:25 Calibrate Now?

..X.. .... 1 | - | Calibration | 07.05 13:25 Calibrated!

..OK.. 1 | - | Calibration | 07.05 13:25 Lab 1 | - | Calibration | 07.05 13:25 Correlation Lab/Meas 0.998726

..OK.. 1 | - | Calibration | 07.05 13:25 Calibration OK

..X.. .... Push .... to start the calibration, push ..X.. to go back one page without calibration. .OK.. takes over the calibration and changes to the next dis-

play. The curve to the left shows the characteristic curve lab vs. measured value.

.... The correlation indicates the average deviation of the charac-

teristic curve from the sample series.

..OK.. As soon as you confirm this prompt, the calibration display appears again; from there you get back to the main menu by pushing four times and you can start the measurement again. DynFAS MW 63 Chapter 4 Calibration 4.5 Adjusting the Calibration A correction factor and an offset factor may be entered later to obtain subsequent adjustment of the calibration (fine cali-

bration). Below please find an example for an offset adjustment. The display to the left appears if you push RUN. The display reading is now compared with the analysis value of the lab sample. The difference has to be entered as offset with the correct algebraic sign. Calculation: Analysis value display = offset Push ESC to return to the main display.

SETUP

CALIBRATION

CALIBRATE CONC DynFAS MW Concentration av. 65.50 %

1 | - | Live Display | 07.05 13:25 Conc av. Conc. act. 64.35%

ESC SAMPLE .. ZOOM 1 | - | Control Unit | 07.05 13:25 Live Display Diagnostic Setup Access Level Language Basic English STOP 1 | - | Setup | 07.05 13:25 Configuration Calibration Input / Output Service Product 1 | - | Calibration | 07.05 13:25 System Adjust Calibrate Conc Advanced 64 Chapter 4 Calibration 1 | - | Calibrate Conc | 07.05 13:25 Sampling Calibr. autom. Tuning View 1 | - | Tuning | 07.05 13:25 Factor Offset 1.00000 0.000 1 | - | Tuning | 07.05 13:25 Offset 0.000 |

ESC ..?.. DEL .... 1 | - | Contro Unit | 07.05 13:25 Live Display Diagnostic Setup Access Level Language Basic English STOP Concentration av. 1 | - | Live Display | 07.05 13:25 Conc av. Conc. act. 64.35%

ESC SAMPLE .. ZOOM 75.50 %

TUNING

OFFSET Enter the calculated offset value, confirm with .... button and push four times to return to the main menu. Select with

LIVE DISPLAY to get back to the display. The reading value should now correspond to the actual value. DynFAS MW 65 Chapter 4 Calibration 4.6 Output of the start-up protocol Datalog Errorlog Info Print Setup 1 | - | Diagnostic | 07.05 13:25 1 | - | Print setup | 07.05 13:25 Print Setup now?

..X.. .... 66 Starting from the main menu, you get to the display to the left by selecting | DIAGNOSTIC | in the Profi mode.

PRINT SETUP Push .... to start the print out by RS 232 and RS 485, push

..X.. to go back one page without sending. The start-up protocol includes all adjustable parameters, calibra-

tion data, data of the system adjust and entries of the sample table. Further information for instance about the format or an ex-

ample of such a protocol can be found in chapter 9.5. DynFAS MW Chapter 5 Password Chapter 5. Password The measuring system can be protected by passwords against unauthorized access. The following access levels are available:

Read only The measuring system cannot be started and stopped. You can only switch from the live display to Diagnostic and to Access Level. Basic On the Basic level you can make essential entries, and stop and start the system. Profi The Profi mode allows additional entries in the process type menu, calibration menu and opens the Service menu. Service The service level is reserved to service personnel. You have to enter a password to change from the access le-

vel Read only to Basic or Profi. At the time of delivery, this password is The password can be changed in the profi mode at: menu |

SETUP | CHANGE PASSWORD. Changing from Profi to Basic or vice versa is possible without password. You can change the password on the Profi or Basic level. PASS1 Tip Depending on the access level, some menu items are hidden. DynFAS MW 67 Chapter 5 Password 5.1 Forgot password The device is in the read only mode and the user forgot the password. In order to carry out a reset of the user level, use the following way:

Switch of the device. Switch it on again, the moment when all 5 LEDs light up while booting the 0 (zero-key) has to be pushed constantly for 8 seconds!

The device boots in basic mode now. Henceforward it can be carried out a manual general reset or define a new pass-

word respectively. IMPORTANT Caution: check your process before switching of the device. For example the power output drop to 0 mA. 68 DynFAS MW Chapter 6 Inputs / Outputs Chapter 6. Inputs / Outputs The measuring system includes two separate floating current outputs. 6.1 Current Outputs 1 | - | Control Unit | 07.05 13:25 Live Display Diagnostic Setup Access Level Language Basic English RUN 1 | - | Setup | 07.05 13:25 Configuration Calibration Input / Output Service Product 1 | - | Inputs/Outputs | 07.05 13:25 Current Output Current Input PT100 Digital Output Digital Input 1 | - | Current Output | 07.05 13:25 Current Out 1 Current Out 2 Current outputs 1 and 2 can be assigned to the concentra-

tions for calibration with two concentrations. You get to the setup display as follows.

SETUP

INPUTS / OUTPUTS

CURRENT OUTPUT Now you can select the respective current output and assign it to the concentration after calibration. DynFAS MW 69 Chapter 6 Inputs / Outputs 6.1.1 Current Output Setup 1 | - | Current Output | 07.05 13:25 Current Out 1 Current Out 2

CURRENT OUT 1 1 | - | Current Out 1| 07.05 13:25 Assignment Upper Value Lower Value Test / Adjust Error current Conc 95.00 %

60.00 %

1 | - | Current Out. 1| 07.05 13:25 Assignment Conc Conc 2 Current In 1 Current In 2 PT100

ASSIGNMENT

CONC Select and confirm with .... ESC ..?.. .... In case of two concentrations and outputs enabled, the assign-

ment can be chosen as needed. 1 | - | Current Out 1| 07.05 13:25 Assignment Upper Value Lower Value Test / Adjust Error current Conc 95.00 %

60.00 %

1 | - | Current Out. 1| 07.05 13:25 Upper value 95.00 |

ESC ..?.. DEL ....

UPPER VALUE Delete the old value with DEL. Enter the new limit value and confirm with .... Set the lower value also as described above. 70 DynFAS MW Chapter 6 Inputs / Outputs 6.1.2 Test and Adjustment Prerequisite: You are in the Profi mode

TEST / ADJUST 1 | - | Current Out 1| 07.05 13:25 Conc 95.00 %

60.00 %

Assignment Upper Value Lower Value Test / Adjust Error current 1 | - | Test / Adjust | 07.05 13:25 Loop test Adjust Live current 1 | - |Adjust Current | 07.05 13:25 Loop should be removed from autmatic control

..X.. .OK. 1 | - |Adjust Current | 07.05 13:25 Connect reference meter

..X.. .OK. 1 | - |Adjust Current | 07.05 13:25 Setting Current Output to 4 mA 4.00 mA

ADJUST Tip Current output 1 can only be set from 4 to 20 mA, since it is foreseen for a HART communicator Push ..OK.. to confirm that the process is not affected by the measurement. Push ..OK.. to confirm that the measuring system is con-

nected. Push ..OK.. to confirm. .X.. .OK. DynFAS MW 71 Chapter 6 Inputs / Outputs 1 | - |Adjust Current | 07.05 13:25 Enter meter value 3.80 mA

ESC DEL .... 1 | - |Adjust Current | 07.05 13:25 4 mA adjusted. .X.. .OK. 1 | - |Adjust Current | 07.05 13:25 Setting Current Output to 20 mA

..X.. .OK. 1 | - |Adjust Current | 07.05 13:25 Enter meter value 19.80 |

mA Read off display of measuring system and enter value. 4 mA value adjusted. Push ..OK.. to confirm. Read off display of measuring system and enter value. ESC DEL .... 1 | - |Adjust Current | 07.05 13:25 20 mA adjusted. .X.. .OK. Adjustment finished. 1 | - | Test / Adjust | 07.05 13:25 Loop test Adjust Live current 15.00 mA 72 To check the current loop and possibly connected remote dis-

plays, you can set a current between 4 and 20 mA via the test function. If you quit the test function, the system automatically switches back to the live current. DynFAS MW Chapter 6 Inputs / Outputs 6.1.3 Error Current Different signal effects can be assigned to the output current. 1 | - | Current Out 1 | 07.05 13:25 Assignment Upper Value Lower Value Test / Adjust Error current Conc 95.00 %

60.00 %

1 | - | Error current | 07.05 13:25 Alarm Mode Value Value 22.00 mA

ERROR CURRENT

ALARM MODE Fixed values, Hold or freely adjustable values between 0 and 24 mA can be assigned. 1 | - | Error current | 07.05 13:25 Alarm Mode 22.00 mA 3.5 mA Hold Value

VALUE With this setting, you can default any current value for the error case. 1 | - | Error current | 07.05 13:25 Value 3.50 mA ESC DEL .... Enter value and confirm with ..... DynFAS MW 73 Chapter 6 Inputs / Outputs 6.1.4 Current Output 2 1 | - | Current Out | 07.05 13:25 Current Out 1 Current Out 2 1 | - | Current Out 2 | 07.05 13:25 Assignment Upper Value Lower Value Conc 2 95.00 %

60.00 %

4 - 20 mA Range Test / Adjust Error current Range 1 | - | Current Out. 2 | 07.05 13:25 0 20 mA 4 20 mA ESC ....

CURRENT OUT 2 All settings for current output 2 have to be made in the same manner as for output 1, with the exception of the range setting.

RANGE After selection of the required range, carry out all setting and calibration steps as described in chapter 6.1.2. 74 DynFAS MW Chapter 6 Inputs / Outputs 6.2 Current Inputs 1 | - | Inputs/Outputs | 07.05 13:25 Current Output Current Input PT100 Digital Output Digital Input If the window below is not displayed, you can invoke it on the main menu via | SETUP |INPUT/OUTPUT |

CURRENT INPUT

CURRENT IN 1 Current In 1 Current In 2 6.2.1 Enabling the Current Input 1 | - | Current In | 07.05 13:25 1 | - | Current In 1 | 07.05 13:25 Enabled Adjust Live current 4.00 mA no

ENABLED

ENABLING 1 | - | Current In 1 | 07.05 13:25 Enabled No Yes The menu ADJUST is only displayed at the profi mode. ESC ..?.. .... If a measurement is running, enabling an adjusted current input which is not used may cause an error. DynFAS MW 75 Chapter 6 Inputs / Outputs 6.2.2 Range Setting and Adjustment Prerequisite: You are in the Profi mode

RANGE SETTING

4 20 mA

ADJUST 1 | - | Current In 1 | 07.05 13:25 Enabled Range Upper value Lower value Adjust Live current yes 0 20 mA 100.00 C 0.00 C 4.00 mA 1 | - | Current Input 1 | 07.05 13:25 Range 0 20 mA 4 20 mA ESC ..?.. .... 1 | - | Current In 1 | 07.05 13:25 Enabled Range Upper value Lower value yes 4 20 mA 100.00 C 0.00 C Adjust Live current 4.00 mA 1 | - |Adjust Current | 07.05 13:25 Loop should be removed from automatic control

..X.. .OK. 1 | - |Adjust Current | 07.05 13:25 Connect current generator

..X.. .OK. Push ..OK.. to confirm that the process is not affected by the measurement. Push ..OK.. to confirm that the current generator is con-

nected. 76 DynFAS MW Chapter 6 Inputs / Outputs 1 | - |Adjust Current | 07.05 13:25 Set current generator to 4 mA. .X.. .OK. 1 | - |Adjust Current | 07.05 13:25 Generator set to 4 mA?

..X.. .OK. 1 | - |Adjust Current | 07.05 13:25 4 mA adjusted. .X.. .OK. Set current generator to 20 mA. 1 | - |Adjust Current | 07.05 13:25

..X.. .OK. 1 | - |Adjust Current | 07.05 13:25 Generator set to 20 mA

..X.. .OK. 1 | - |Adjust Current |07.05 13:25 20 mA adjusted.

Set current generator to 4 mA. Push the ..OK.. button to confirm. Push ..OK.. to confirm adjustment of the lower value.

Set current generator to 20 mA. Push the ..OK.. button to confirm. Push ..OK.. to confirm adjustment of the lower value. .X.. .OK. DynFAS MW 77 Chapter 6 Inputs / Outputs Adjustment finished. The live current is displayed. If necessary, carry out range setting and calibration of current input 2 as described above.

Pt 100

ENABLED 1 | - | Current In 1 | 07.05 13:25 yes 4 20 mA 100.00 C 0.00 C Enabled Range Upper value Lower value Adjust Live current 4.00 mA 6.3 Pt 100 6.3.1 Pt 100 Enabling 1 | - | Inputs/Outputs | 07.05 13:25 Current Output Current Input PT100 Digital Output Digital Input 1 | - | Pt 100 | 07.05 13:25 no Enabled Adjust Pt 100 live The menu ADJUST is only displayed at the profi mode. 1 | - | Pt 100 | 07.05 13:25 Enabled no yes ESC ..?.. .... Select yes and pushc.. to confirm. 78 DynFAS MW Chapter 6 Inputs / Outputs 6.3.2 Pt 100 Calibration Prerequisite: You are in the Profi mode 1 | - | Pt 100 | 07.05 13:25 Enabled yes Adjust Pt 100 Live

ADJUST 1 | - | Adjust Pt100 | 07.05 13:25 Connect 100 Ohm resistor to Pt100 terminals.

(for 0C/31.4F adjustment)

..X.. .OK. .OK.. 1 | - | Adjust Pt100 | 07.05 13:25 100 Ohm resistor connected?

..X.. .OK. 1 | - | Adjust Pt100 | 07.05 13:25 Lower point adjusted. .X.. .OK. 1 | - | Adjust Pt100 | 07.05 13:25 Connect 138.5 Ohm resistor to Pt100 terminals.

(for 100C/211.4F adjustment)

..X.. .OK. Connect 100 Ohm resistor to Pt100 terminals [11] [23]. Confirm once more with ..OK... Adjustment of lower point finished. After connection of the resistor, confirm with ..OK... DynFAS MW 79 Chapter 6 Inputs / Outputs 1 | - | Adjust Pt100 | 07.05 13:25 138.5 Ohm resistor connected?

..X. .OK. Upper point adjusted. 1 | - | Adjust Pt100 | 07.05 13:25

..X.. .OK. 6.4 Digital Output Confirm safety prompt. Calibration is finished. The measuring system includes two changeover relay outputs which can be assigned to the respective application. Relay 1 is associated with LED signal 1 and relay 2 with signal 2. 6.4.1 Digital Output Assignment 1 | - | Digital Output | 07.05 13:25 Relay 1 Relay 2 Test 1 | - | Relay 2 | 07.05 13:25 None Function From the main menu you get to the display depicted to the left via | Setup | Input/Output | Digital Output

Relay 2 Select the display with the arrow keys. 80 DynFAS MW Chapter 6 Inputs / Outputs 1 | - | Relay 2 | 07.05 13:25 Function None Error Hold meas. No product Alarm min Alarm max ESC ..?.. .... 6.5 Digital Input Push and then .... to assign a function to the relay. Function Description None Error Hold No product Alarm min. Alarm max. Relay and LED function disabled In case of error, relay and LED will be set. If Hold function is enabled, relay and LED will be set. If Pause detection is enabled, this will be signaled via relay and LED. The relay switches if the value falls below the limit value to be set. The relay switches if the value exceeds the limit value to be set. Different functions can be assigned to the digital inputs. See table below. Function1 Function2 Function3 Terminals DI 1 DI 2 None None Start/Stop Hold Product 12/24 13/25 None 14/26 Sample Product DI 3 For external start function, the start function has to be set to external in the Measurement menu window. Hold: averaging is stopped, but the measurement continues to run. Sample: sampling is started by closing the contact. Product: by closing the contact it changes into another product (product 1 to 4). Details see chapter 6.5.1. DynFAS MW 81 Chapter 6 Inputs / Outputs 6.5.1 External Product Selection 1 | - | Digital Input | 07.05 13:25 Status DI 1 Function DI 2 Funktion DI 3 Function None None None 1 | - | Digital Input | 07.05 13:25 DI 2 Function None Hold Product From the main menu you get to the window display depicted to the left via | SETUP | INPUT/OUTPUT | DIGITAL INPUT.

DI 2 FUNCTION

PRODUCT ESC ..?.. .... To change all 4 products, DI 3 also has to be set to product. Please take the terminal assignment from the table below. 1 | - | Digital Input | 07.05 13:25 Status DI 1 Function DI 2 Function DI 3 Function None Product None Terminals Product 1 Product 2 Product 3 Product 4 DI 2 13 / 25 open closed open closed DI 3 14 / 26 open open closed closed Caution!

If you select a product for the first time (product 2 to 4) all adjustments and contents of the resent product are copied into the new one, including:

- Configuration data

- System calibration

- Calibration data (including sampling table)

- Input/Output definitions 82 DynFAS MW Chapter 7 Factory Settings Chapter 7. Factory Settings This function allows you to reset the measuring system to its original status (see chapter 9. Factory Settings). Prerequisite: You are in the Profi mode. 1 | - | Control Unit | 07.05 13:25 Live Display Diagnostic Setup Access Level Language RUN 1 | - | Setup | 07.05 13:25 Configuration Calibration Input / Output Service Product Change password 1 | - | Service | 07.05 13:25 Factory settings General reset Memory Tool Data printout HART interface

SETUP

SERVICE

FACTORY SETTINGS 1| - | Factory Settings| 07.05 13:25 Restore now?

..X.. .... If you confirm this prompt, all parameters and configuration set-

tings will be reset to their original status, with the exception of the sampling table and the reference measurement. DynFAS MW 83 Chapter 8 Error Lists Chapter 8. Error Lists 8.1 Error Lists 8.1.1 Hardware Error 8.1.2 Input Error The status of the device is signalized by LEDs. After the error has been remedied, the LEDs are reset to the normal status. Code Error 14 Battery voltage 20 21 39 HF temperature out of range Attention: Ambient temperature too high!

RF hardware fail-

ure Possible cause Battery is nearly empty, replace immediately. See Hardware Manual, chapter 5.4 Battery. Check the operating tempera-

ture of the control unit, allow-

able range: -20 to +60 C Check the operating tempera-

ture of the control unit, allow-

able range: -20 to +60 C Faulty cable connections be-

tween mother board and HF-

module. Check the plug on the motherboard. Caution: disconnect the evalua-

tion unit from the mains before-

hand!

For all other error message, please contact the service de-

partment from BMA Schaltanlagen. Error Value too large Value too small Table is empty Probable Cause Input value too large Input value too small Sampling has been selected without previous sample measurement Chart data faulty The measuring system has determined No chart data available Sampling full faulty chart data during calibration. The calculated chart data have been de-

leted or calibration has not been com-

pleted. You have tried to measure more then 20 samples. DynFAS MW 85 Chapter 8 Error Lists 8.1.3 Measurement Error and Error Prompts Code Error 50 52 53 54 55 60 61 62 70 71 80 81 Sigma of phase is too large Attenuation too high No product No system calibration done Insertion attenua-

tion is not reached Current input 1 out of range Current input 2 out of range Pt 100 tempera-

ture out of range Concentration out of range Concentration 2 out of range Current output 1 out of range Current output 2 out of range Possible cause The measured phase exceeds the permissible limit value. The measured attenuation ex-

ceeds the permissible max. value. The evaluation unit is in pause mode (no product is signaled). No system calibration has yet been carried out. Details see chapter 4.2 The enabled current input has not yet been calibrated or is not occupied. The enabled current input has not yet been calibrated or is not occupied. The enabled Pt 100 input has not yet been calibrated or is not occupied. The concentration calculated on the basis of the raw data is out-

side the valid measuring range. The concentration calculated on the basis of the raw data is out-

side the valid measuring range. The concentration calculated on the basis of the current is out-

side the current range. The concentration calculated on the basis of the current lies out-

side the current range. 86 For all other error message, please contact the service de-

partment from BMA Schaltanlagen. After the measurement error is remedied, the measurement re-

turns into the status before error. There is no confirmation nec-

essary. DynFAS MW Chapter 9 Calibration Data Sheet Chapter 9. Calibration Data Sheet 9.1 Configuration 9.1.1 General Data General Data Date Time Tag Factory setting actual actual

Setup 9.1.2 Measurement Measurement Meas. mode Start mode Averaging Reset averaging Factory setting continuous keyboard 20 no Setup 9.1.3 Plausibility Plausibility Process limits Phase measurement Sigma Phi/att ratio Auto set Pause detection Factory setting 50.0 100.0 100.00 6.0 OFF no

-15.0 dB Setup 9.1.4 Microwave Microwave Cable Ref. cable length Signal cable length Factory setting 4.00 m 4.00 m Setup 9.2 Product Product Product Factory setting 1 Setup DynFAS MW 87 Chapter 9 Calibration Data Sheet 9.3 Inputs/Outputs 9.3.1 Current Output Current out 1 Assignment Upper value Lower value Test/Adjust Error current Current out. 2 Assignment Upper value Lower value Range Test/Adjust Error current 9.3.2 Current Input Current in 1 Enabled Range Upper value Lower value Adjust Current in2 Enabled Range Upper value Lower value Adjust Factory setting Setup Conc. 95.00 60.00 O.K. Hold Factory setting Setup Keine 95.00 60.00 4 20 mA O.K. Hold Factory setting Setup no 4 20 mA 100.00 0.00 O.K. Factory setting Setup no 4 20 mA 100.00 0.00 O.K. 9.3.3 Pt 100 Input Pt 100 Enabled Pt 100 Adjust Factory setting Setup no O.K. 9.3.4 Digital Output Digital output Relay 1 Relay 2 Factory setting Setup Error Hold 88 DynFAS MW Chapter 9 Calibration Data Sheet 9.3.5 Digital Input Digital input DI 1 function DI 2 function DI 3 function Factory setting Setup none none none 9.4 Calibration Data 9.4.1 Calibration Coefficients Calibration Calibration order Calibration basic Coefficients A1 A2 B1 B2 C Compensation Mode Order Ref. temp. TC_Phi 1 TC_Phi 2 TC_Attn 1 TC_Attn 2 Factory setting Setup linear Phase

-0.19 0.0 0.0 0.0 75.00 none additive linear 0.00 0.00000 0.00000 0.00000 0.00000 9.4.2 Typical Calibration Coefficients Concentration value at system calibration C:

For applications with the container probe A1:

-0.19 for determination of the concentration or dry matter substance (Brix-content). DynFAS MW 89 Chapter 9 Calibration Data Sheet 9.5 Start-up protocol printout Output is possible by using RS 232 and RS 485. The output is started under menu | DIAGNOSTIC | PRINT SETUP |. The serial interfaces RS 232 and RS 485 have the following accesses:

Data transfer rate 38400 Bd, 8 data bits, no parity, 1 stop bit. The protocol will be saved via a terminal program into a TXT-

file. To display it e.g. via Excel the following data format has to be regarded:

Separators:

Decimal-separator:

1000-separator:

The following code-list is for the interpretation of the start-

up protocol; see an example of a protocol in chapter 9.5.1. Parameter tabulator

, Information Log type Log time Measuring mode Start mode Compensation input Code-

No. 0 1 2 3 0 1 2 3 4 5 0 1 0 1 0 1 2 3 Log type:

Disabled Single Continuous Stop on error Log time:

15 Minutes 1 Hour 4 Hours 8 Hours 1 Day 3 Days Meas. mode:

Continuous Batch Start mode (Start/Stop):

Keypad Extern Compensation input:

None Current In 1 Current In 2 PT100 90 DynFAS MW Chapter 9 Calibration Data Sheet Parameter Calibration mode Calibration variable Compensation mode Compensation fit Measure con-

figuration AO Assign Code AO Alarm select code Range selec-

tion AI Range se-

lection AI Enabled[2]

DO Function DO Assign-

ment Code-

Nr. 0 1 0 1 2 0 1 0 1 0 1 2 0 1 2 3 4 5 0 1 2 3 0 1 0 1 0 1 2 3 4 5 0 1 2 3 4 Information Cal. order:

Lineare regression Quadratic regression Cal. base:

Phase Attenuation Both (Phase and Attenuation) Compensation mode:

Additive Multiplicative Compensation order:

Lineare regression Quadratic regression Process type:

1 Concentration 2 Concentrationen Split Concentration Assignment of current output:

None Concentration Concentration 2 Current In 1 Current In 2 PT100 Error current for current output:

22 mA 3.5 mA Hold Value Current output range:

0 20 mA 4 20 mA Current input range:

0 20 mA 4 20 mA State current in 2, enabled yes/No Relay function:

None Error Hold meas. No product Alarm min Alarm max Relay: the min/max alarm is as-

signed to :

Concentration Concentration 2 Current In 1 Current In 2 PT100 DynFAS MW 91 Chapter 9 Calibration Data Sheet Parameter DI Function selection Printout mode Access level Language Code-

Nr. 0 1 2 3 4 0 1 2 3 0 1 2 3 0 1 2 Information Function of digital inputs:

None Start/Stop Hold Sample Product Form of data printout:

Disabled Line Table Line + Table Access level:

Read only Basic Profi Service Language:

English German French 92 DynFAS MW Chapter 9 Calibration Data Sheet Examples of a start-up protocol Interpretation:

( * Only relevant for service) Product1 Product2 Prod.3 Prod.4 1 2 2 45.3 C 46.7 C 8.94 V

Control Unit 8005 1005 000-000 1.00 02.06.2009 Start of Setup:

Entry Log type :

Log time :

Number of errors :

NTC temperature :

max. NTC temperature :

9V power supply :

Tag :

Device Type :

Unique device ID number :

Serial number :

Final assembly number :

Software version :

Software release date :

Actual date :

Actual time :

9.5.1 Examples of a start-up protocol Menu:

Product Datalog Info Measurement Measuring mode :

Plausibility Microwave Marker Start mode :

Filter damping value :

Filter damping value[2] :

Filter damping value[3] :

Reset average :

Lower limit :

Upper limit :

Max. phase sigma :

Correlation Phi/Att :

Auto-set mode :

Pause detection :

Minimum attenuation :

Ref. cable length :

Meas. cable length :

Wave band selection :

Start frequency :

Internal Attenuation :

Marker name :

Marker value :

Marker name[2] :

Marker value[2] :

Nbr of sweeps for reference:

21.07.2009 12:18 0 0 20 20 20 FALSE 0 100 100 6 FALSE FALSE

-15.0 dB 4.00 m 4.00 m 1 2 0 Mark1 50 Mark2 50 10 System adjust See code-list See code-list Number of entries into errorlog

Record date Record time See code-list See code-list Number of average values

Min. Concentration Max. Concentration Sigma max. Phi/Att ratio Auto set: ON/OFF

For Concentration For Concentration For Concentration 2 For Concentration 2 DynFAS MW 93 Chapter 9 Calibration Data Sheet Calibrate concentration Calibrate concentration 2 Advanced Compensation input :

Compensation reference :

Calibration mode :

Calibration variable :

Phase coefficients :

Phase coefficients[2] :

Attenuation coefficients :

Attenuation coefficients[2] :

Constant coefficient :

Compensation mode :

Compensation fit :

Compensation reference :

Phase coeff. for comp. :

Phase coeff. for comp.[2] :

Attenuation coeff. for comp :

Attenuation coeff. for comp[2]

Adjust factor :

Adjust offset :

Compensation input :

Compensation reference :

Calibration mode :

Calibration variable :

Phase coefficients :

Phase coefficients[2] :

Attenuation coefficients :

Attenuation coefficients[2] :

Constant coefficient :

Compensation mode :

Compensation fit :

Compensation reference :

Phase coeff. for comp. :

Phase coeff. for comp.[2] :

Attenuation coeff. for comp :

Attenuation coeff. for comp[2]

Adjust factor :

Adjust offset :

Tara Phase (/GHz) :

Tara Attenuation (dB) :

Measure configuration :

Range split value :

0 0 0 0

-0.19 0 0 0 50 0 0 0 0 0 0 0 1 0 0 0 0 0

-0.19 0 0 0 50 0 0 0 0 0 0 0 1 0 0.00

/GHz 0.00 dB 0 75 See code-list See code-list See code-list A1 A2 B1 B2 C See code-list See code-list C_Ph1 C_Ph2 C_dB1 C_dB2 See code-list See code-list See code-list A1 A2 B1 B2 C See code-list See code-list C_Ph1 C_Ph2 C_dB1 C_dB2 Process type: see code-list Split value 94 DynFAS MW Chapter 9 Calibration Data Sheet Current out 1 Current out 2 Current in 1 Current in 2 PT100 input Relay 1 Relay 2 Digital input AO Assign code :

AO Upper range value :

AO Lower range value :

AO Current value :

AO Alarm select code :

AO Error current value :

AO Assign code[2] :

AO Upper range value[2] :

AO Lower range value[2] :

Range selection[2] :

AO Current value[2] :

AO Alarm select code[2] :

AO Error current value[2] :

AI Enabled :

AI Range selection :

AI Upper range value :

AI Lower range value :

AI Current :

AI Enabled[2] :

AI Range selection[2] :

AI Upper range value[2] :

AI Lower range value[2] :

AI Current[2] :

AI Enabled[3] :

Pt100 value :

DO Function :

DO Assignment :

DO Threshold :

DO Hysteresis :

DO Function[2] :

DO Assignment[2] :

DO Threshold[2] :

DO Hysteresis[2] :

DI Function selection :

DI Function selection[2] :

DI Function selection[3] :

Printout mode :

Access level :

Language :

End of Setup 1 100.00%

0.00%

4.00 mA 2 22.00 mA 0 100 0 1 4.00 mA 2 22.00 mA FALSE 1 100 0 0.00 mA FALSE 1 100 0 0.02 mA TRUE 2.8 C 1 0 0.00%

5.00%

2 0 0.00%

5.00%

0 0 0 1 2 1 Assignment: see code-list Upper value Lower value Live current Error current: see code-list Error current value Assignment: see code-list Upper value Lower value Range Live current Error current: see code-list Error current value Range: see code-list Upper value Lower value Live current Range: see code-list Upper value Lower value Live current Live value Function: see code-list Assignment: see code-list

Function: see code-list Assignment: see code-list

Function digital input 1 Function digital input 2 Function digital input 3 DynFAS MW 95 Chapter 9 Calibration Data Sheet Start of Reference Data Product 1:

Mean Atten.:

Phase at fm:

Phase offset:

Phase slope:

Phase sigma:

Frequency[GHz]

2.42 2.43 2.44 2.45 2.46 46.8509 dB 42.6285 deg/GHz

-825.586 deg 380.984 deg/GHz 0.24575 Phase[Deg] Atten.[dB]

96.41 100.71 103.08 108.12 111.75 46.2 46.8 47.13 46.84 47.28 System adjustment data:

Sample Table Start of Sample Data:

Product 1: Sample Data for Concentration 1:

Sample:

1|16.03 - 20:53 2|17.03 - 00:22 Correlation factor between lab and meas values:

End of Sample Data Do not use following data!

Active:

TRUE TRUE 1 Kon.(%): Lab.(%): AIN1(C): AIN2(C): Temp.(C): Phi.(/GHz): Att.(dB):

50.0193

-0.16 0.18 50.1061

-0.1

-0.56 2.83 2.71 0 0 0 0 0 0 96 DynFAS MW Chapter 9 Calibration Data Sheet 9.6 Sample Table No. Active Measured Lab value Current In 1 Current In 2 Pt 100 Phi (m) Attenua-

value tion 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 98 DynFAS MW Notes DynFAS MW 99 Notes 100 DynFAS MW